M. HNIZDIL, P. KOTRBACEK: HEAT TREATMENT OF RAILS 329–332 HEAT TREATMENT OF RAILS TOPLOTNA OBDELAVA TIRNIC Milan Hnizdil, Petr Kotrbacek Brno University of Technology, Faculty of Mechanical Engineering, Heat transfer and fluid flow laboratory, Technicka 2896/2, 616 69, Brno, Czech Republic hnizdil@fme.vutbr.cz Prejem rokopisa – received: 2015-12-23; sprejem za objavo – accepted for publication: 2016-03-31 doi:10.17222/mit.2015.357 Heat treatment is increasingly used in the heavy industry. The main advantage of this method is the achievement of the required material and mechanical properties. Heat treatment allows for a manufacturing process, which can improve product performance by increasing the steel strength, hardness and other desirable characteristics. The microstructure, grain size and chemical composition of steel affect its overall mechanical behavior. Heat treatment is an efficient way to manipulate the properties of a steel product by controlling the cooling rate. It can be expressed using the heat-transfer coefficient (HTC). The controllability of the cooling process is very important. Mist and water nozzles may provide good controllability of the HTC. An experimental stand was designed and built. The stand consists of a movable trolley with a test sample, which moves under a spray at a given velocity. Sensors record the temperature history of the tested material. This experimental stand enables simulations of a variety of cooling regimes and evaluations of the final structures of tested samples. The same experimental stand is also used for designing cooling sections in order to determine the required heat-treatment procedures and the final structures. This paper describes a cooling-section design procedure for obtaining the required structure and mechanical properties of rails. Keywords: heat transfer, heat treatment, cooling, heat-transfer coefficient, spray cooling Uporaba toplotne obdelave se v te`ki industriji pove~uje. Glavna prednost te metode je, da se dose`e zahtevane mehanske lastnosti materiala. Toplotna obdelava omogo~a postopke izdelave, ki lahko izbolj{ajo lastnosti proizvodov s tem, da pove~ajo trdnost jekla, trdoto in druge za`eljene zna~ilnosti. Mikrostruktura, velikost zrn in kemijska sestava jekla vplivajo na mehanske lastnosti. Toplotna obdelava je u~inkovita pot za vplivanje na lastnosti jeklenega proizvoda s kontroliranjem hitrosti ohlajanja. Lahko se jo izrazi z uporabo koeficienta prenosa toplote. Mo`nost kontrole postopka ohlajanja je zelo pomembna. Obvladanje procesa ohlajanja je zelo pomembno. Vodna para in vodne {obe omogo~ajo dobro kontrolo koeficienta prenosa toplote (angl. HTC). Na~rtovano in postavljeno je bilo eksperimentalno stojalo. Stojalo sestoji iz vozi~ka z vzorcem, ki se pomika pod {obe z dano hitrostjo. Senzorji bele`ijo temperaturno zgodovino vzorca. Eksperimentalno stojalo omogo~a simulacijo razli~nih re`imov ohlajanja in oceno kon~ne mikrostrukture preizku{enega vzorca. Isto stojalo je uporabno tudi kot orodje pri na~rtovanju hladilnih odsekov za dolo~anje postopka toplotne obdelave in kon~ne mikrostrukture. ^lanek opisuje postopek na~rtovanja odseka za izvajanje hlajenja, za zagotavljanje `eljene mikrostrukture in mehanskih lastnosti `elezni{kih tirnic. Klju~ne besede: prenos toplote, toplotna obdelava, ohlajanje, koeficient prenosa toplote, ohlajanje s pr{enjem 1 INTRODUCTION Heat treatment of rolled materials by hot rolling plants has become frequent. Alloying elements are typi- cally used to improve material properties. Heat treatment is a different approach applied to achieve the required material properties using fewer alloys in the steel. Heat treatment enables the manufacture of modern steels with a higher ratio of yield strength and elongation. The con- trollability of the cooling process is the most important aspect for achieving the required mechanical properties. An appropriate cooling intensity and its duration are chosen with respect to the continuous cooling transfor- mation diagram (CCT) for the selected material. Numerical simulation of the cooling follows. One task is to determine the boundary condition (HTC – heat trans- fer coefficient) for the simulation because various para- meters such as nozzle type, spray distance, water impingement density, nozzle position, nozzle overlap, movement velocity and scales have significant influences on the cooling intensity.1–3 Additionally, accurate ther- mo-physical material properties are needed for simu- lations.4 The Heat Transfer and Fluid Flow Laboratory developed a methodology for predicting the temperature field of heat-treated rails. This methodology is described in this article. 2 DESIGN STRATEGY FOR THE COOLING SECTION Three different types of experiments were done to predict the required cooling regime defined by the CCT diagram. A special hardening-capacity test bench (Fig- ure 1) was developed to find the limits of a quenched rail. The test bench consists of a heater, a trolley with a tested sample, a water nozzle holder and a pneumatically driven deflector. Each test starts with heating a rail-head sample to the initial temperature. This temperature is held for more than 10 min to attain the austenite structure of the entire body. The sample is protected with an inert atmosphere in the furnace to prevent the development of scales. Next, the sample is moved from the heater to a position Materiali in tehnologije / Materials and technology 51 (2017) 2, 329–332 329 MATERIALI IN TEHNOLOGIJE/MATERIALS AND TECHNOLOGY (1967–2017) – 50 LET/50 YEARS UDK 621.78:66.017:669.14.018.298 ISSN 1580-2949 Professional article/Strokovni ~lanek MTAEC9, 51(2)329(2017) under the nozzle. The pneumatically driven deflector, positioned between the nozzle and the sample, is moved and the water sprays the top of the rail head. Each sample is equipped with thermocouples under the surface to detect the temperature gradient in the material. The material hardness and its structure are observed. The hardness values of the original (base) material and the heat-treated material are compared because the heat- treatment process is dependent on the quality of the steel-making process (chemical composition, enclosures, casting speed, etc.).5–8 If these tests are sufficient, heat-transfer tests are then performed. A special testing bench called a linear stand (Figure 2) was developed by the Heat Transfer and Fluid Flow Laboratory. This bench is a six-meter long girder with a trolley which can move the tested rail sample, plate, etc., through the cooling section. A 25 mm thick, flat austenitic steel plate is used for the heat-transfer tests. It is embedded with four thermocouples positioned 0.5 mm under the sprayed surface. This plate is moved through the spray-cooling system (2 m long) in two directions, forward and backward. The dependences of the heat-transfer coefficient on the surface temperature are evaluated for various cooling parameters (spray distance, type of nozzle, water im- pingement density, etc.). The obtained boundary condi- tions are used for simulations to predict the temperature field in the rail head. The shape of the rail also has a significant influence on the cooling intensity. Therefore, an authentically shaped austenitic steel sample is made and embedded with several thermocouples, positioned 2 mm under the rail surface. The length of this sample is around 300 mm. Simulations of the rail cooling are compared with the temperatures measured during the austenitic rail cooling. The boundary conditions obtained from the flat austenitic steel plate are adjusted and the model is verified with measurements. The last step is the verification including a full-scale, carbon-rail sample. A sample is fixed on the trolley (the linear stand) and moved through the cooling section. The measured and simulated temperatures are compared and the cooling model is verified. Finally, the hardness is measured again. This is the most important result that shows if the cooling regime works optimally. 3 RESULTS The cooling strategy was described in Section 2. The experimental steps began with the study of CCT diagrams. Material R260 was chosen for the heat-treat- ment tests. The hardness-capacity tests were performed first to find the limit of the quenched material and to choose the appropriate nozzle size with respect to the required cooling regime. All the tested samples were embedded with thermocouples to verify the cooling regime. These samples were sawed after quenching and hardness was measured along the center line of the rail head (from the top of the surface down to the center – the red line). An example of the cooling regime (for a successful test) is shown in Figure 3. The measured hardness for this sample was around 400 HV0.3 (Figure 4). The required fine pearlite struc- ture was found using a microstructure analysis (Figure 5). M. HNIZDIL, P. KOTRBACEK: HEAT TREATMENT OF RAILS 330 Materiali in tehnologije / Materials and technology 51 (2017) 2, 329–332 MATERIALI IN TEHNOLOGIJE/MATERIALS AND TECHNOLOGY (1967–2017) – 50 LET/50 YEARS Figure 1: Hardening-capacity test bench Slika 1: Preizku{anje zmogljivosti utrjevanja Figure 3: Temperature record for the rail head during a successful static-hardness-capacity test Slika 3: Zapis temperature glave tirnice med uspe{nim preizkusom zmogljivosti trdote Figure 2: Linear-stand scheme Slika 2: Shema linearnega stojala An appropriate choice of the nozzle and the verifi- cation of the cooling regime using the CCT diagram were confirmed with a static-hardening-capacity test. The next step was to find the cooling parameters for the moving samples (transient boundary conditions). The linear stand was used for these tests. A 25 mm thick, flat austenitic steel plate was used and several parameters such as water pressure, spray distance, spray angle and movement velocity were tested. The boundary conditions obtained from the experiment were used to simulate the cooling regime for a real moving rail. A full-scale rail sample (material R260) was built and embedded with six thermocouples positioned 2 mm under the surface (Fig- ure 6). M. HNIZDIL, P. KOTRBACEK: HEAT TREATMENT OF RAILS Materiali in tehnologije / Materials and technology 51 (2017) 2, 329–332 331 MATERIALI IN TEHNOLOGIJE/MATERIALS AND TECHNOLOGY (1967–2017) – 50 LET/50 YEARS Figure 4: Measured hardness of the rail head after the static-hard- ness-capacity test Slika 4: Izmerjena trdota v glavi tirnice med stati~nim preizkusom trdote Figure 7: Temperature record for the heat-treated full-scale sample Slika 7: Temperatura zabele`ena na toplotno obdelanem realnem vzorcu Figure 5: Microstructure – close to the sprayed surface – center of the rail-head surface Slika 5: Mikrostruktura – blizu po{kropljene povr{ine – sredina po- vr{ine glave tirnice Figure 8: Measured hardness at the center line of the rail head Slika 8: Trdota izmerjena na sredini glave tirnice Figure 6: Full-scale carbon sample heated to the initial temperature before entering the cooling section Slika 6: Realen vzorec ogret do za~etne temperature pred vstopom v podro~je ohlajanja The first full-scale test showed that the rail shape has a significant influence on the cooling intensity, so additional experiments with a full-scale austenitic sam- ple and temperature-field prediction-model tuning were necessary to obtain the required material structure. Finally, a full-scale, carbon-rail sample was made and it too was embedded with thermocouples. Simulated tem- peratures were compared to measured temperatures and the model was verified. An example of the cooling re- gime of a successful full-scale test is shown in Figure 7. The measured hardness of this sample was around 400 HV0.3 (Figure 8). This corresponded to the results from the static-hardening-capacity test. 4 CONCLUSION The goal of this article was to illustrate a verified methodology for rail heat treatment. The first step was to compute a CCT diagram and determine the settings for the optimum cooling regime to achieve the required material structure. The accuracy of the CCT diagram was verified with a hardening-capacity test (Jominy test). The next step was to measure the dependence of the heat- transfer coefficient on the surface temperature using a flat austenitic steel plate with thermal sensors. Various cooling parameters were tested: water pressure, spray distance, spray angle, movement velocity and others. These boundary conditions were used to predict the tem- perature-field evolution in the rail. It was found that the rail shape has a significant influence on the cooling in- tensity. A full-scale austenitic steel rail sample (300 mm long) was made and the cooling model was tuned using simulation data and the temperatures measured during the experiments with a full-scale sample. The final design of the cooling section was made and the cooling model was verified by measuring an authentic full-scale carbon sample in the laboratory. The final hardness of the heat-treated rail sample was measured and compared with the data obtained during the hardening-capacity test. Both of these results were around 400 HV0.3. A fine perlite structure was found along the center line of the heat-treated rail-head sample. 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