K. ANGANAN et al.: EXPERIMENTAL STUDY AND ANALYSIS OF THE WEAR PROPERTIES OF ... 201–205 EXPERIMENTAL STUDY AND ANALYSIS OF THE WEAR PROPERTIES OF FRICTION-STIR-WELDED AA7075-T6 AND A384.0-T6 DISSIMILAR ALUMINIUM ALLOYS OF BUTT JOINTS EKSPERIMENTALNA [TUDIJA IN ANALIZA OBRABE ZVAROV, IZDELANIH Z ROTACIJSKIM TORNIM VARJENJEM RAZNOVRSTNIH ZLITIN AA7075-T6 IN A384.0-T6 Karuppannan Anganan1, Subramaniam Prabagaran2, Mayakrishnan Muthukrishnan3 1Karpagam Academy of Higher Education, Coimbatore, Department of Mechanical Engineering, 641 021 Tamil Nadu, India 2Karpagam Academy of Higher Education, Department of Mechanical Engineering, Coimbatore, 641 021 Tamil Nadu, India 3Kalaignar Karunanidhi Institute of Technology, Department of Mechanical Engineering, Coimbatore, 641 402 Tamil Nadu, India anganan09@gmail.com Prejem rokopisa – received: 2017-07-06; sprejem za objavo – accepted for publication: 2017-10-11 doi:10.17222/mit.2017.109 The wear is one of the main issues in friction-stir welding (FSW) of dissimilar aluminium alloys. Two dissimilar metals welded with FSW have different mechanical, metallurgical and chemical properties compared to the parent materials. Therefore, the wear resistance is an important property in an FSW process. In this research, AA7075-T6 and A384.0-T6 aluminium alloys with a thickness of 6.35 mm were selected and a design matrix was developed to produce FSW welds using the MINITAB-17 software. Friction-stir-welded pieces were made as test specimens and their ultimate tensile strengths (UTSs) were tested. In these experiments, the maximum- and minimum-UTS specimens were used for a wear-resistance analysis and its results were compared with the wear resistance of the parent metals. The results were obtained by keeping the revolutions per minute (min–1), time and sliding velocity as constants, while varying the load applied. The rpm, time and sliding velocity were 500, 300 s and 3.141 m/s, respectively. The loads applied were (20, 40 and 60) N. The conclusion is that, under all the applied loads, the wear of the friction-stir weld produced is lower than that of the A384.0-T6 aluminium base metal. On the other hand, the wear of the weld is higher than the AA7075-T6 aluminium base metal. Keywords: wear resistance, dissimilar aluminium alloys, friction-stir welding, base metals, wear-resistance parameters Obraba raznovrstnih aluminijevih zlitin je ena od glavnih tem v raziskavah na podro~ju rotacijskega tornega varjenja (FSW; angl.: Friction Stir Welding). Dve razli~ni kovini, ki ju varimo, imata med FSW razli~ne mehanske, metalur{ke in kemi~ne lastnosti v primerjavi s sorodnimi materiali. Odpornost proti obrabi je pomembna lastnost v FSW-procesu. V tej raziskavi so avtorji izbrali dve Al zlitini AA7075-T6 in A384.0-T6 debeline 6,35 mm in z njima oblikovali matrico za FSW-zvare z uporabo programske opreme MINITAB-17. Izdelali so vzorce varjene s postopkom FSW in dolo~ili natezno trdnost zvarov. Nato so za nadaljnje preiskave obrabe izbrali vzorce z najmanj{o in najve~jo natezno trdnostjo in jih primerjali z FSW-zvari, izdelanimi iz sorodnih materialov. Med eksperimenti so dr`ali konstantne naslednje procesne parametre varjenja: {tevilo obratov na minuto (500 min–1), ~as (300 s) in hitrost drsenja (3,141 m/s); spreminjali pa so obremenitev (20, 40 in 60) N. Avtorji so v tej raziskavi ugotovili, da je obrabna obstojnost zvarov, izdelanih z FSW druga~na od obrabe zvarov izdelanih iz osnovne Al zlitine A384.0-T6 pri vseh obremenitvah. Obrabna obstojnost izdelanih zvarov iz izbranih nesorodnih zlitin pa je primerljiva z zvari izdelanimi iz Al zlitine AA7075-T6. Klju~ne besede: odpornost proti obrabi, raznovrstne Al zlitine, rotacijsko torno varjenje, osnovne kovine, parametri obrabne odpornosti 1 INTRODUCTION FSW is one of the solid-state fumeless welding techniques. It was invented, developed and patented in 1991 by Wayne Thomas, The Welding Institute, United Kingdom.1 For our experiment, the plates to be welded were placed adjacent to each other and tightly clamped by a specially made fixture. A tool was fitted to a chuck and that was then fitted to the spindle of an FSW machine. Figure 1 depicts the FSW machine. A rotating tool with an axial pressure force and longitudinal movement was inserted between the two plates. Hence, as a stirring action takes place between the plates, heat is developed and the metals are plastically deformed and joined together.2 The concept of an FSW process is shown in Figure 2. After the FSW process, the mecha- nical, metallurgical, thermal and chemical properties are changed compared to the parent-material properties. In this research, the wear properties were analysed. L. Guo et al.3 investigated the lubrication effect of annealed Fe78Si9B13 glass particles in the FSW of the AA6061 metal and found that the particles play an important role in improving the wear resistance. S. K. Naimuddin et al.4 conducted an experimental study analysis of similar and dissimilar joints of the materials of (AA6061-AA6061), (AA6082-AA6082) & (AA6061-AA6082) under T6 conditions to find the wear behaviours. They found low wear and low wear resis- tance in the FSW welds. A. M. Hassan et al.5 experimen- tally studied the wear characteristics of aluminium- Materiali in tehnologije / Materials and technology 52 (2018) 2, 201–205 201 UDK 620.1:620.178.16:669.715 ISSN 1580-2949 Original scientific article/Izvirni znanstveni ~lanek MTAEC9, 52(2)201(2018) matrix composites reinforced with graphite and silicon carbide particles using FSW techniques. The results showed that the process parameters greatly influenced the wear resistance of the welded joints. S. Prabagaran et al.7 experimentally proved that the formation of the oxides at the interface plays a signifi- cant role in reducing the wear rate. To take decisions about FSW weld quality, many welding parameters like tool rotational speed, welding feed, axial load, tool pin profile, etc., are considered.8 Many researchers are very interested in optimizing the FSW process parameters.9 At the same time, most of the researchers analyse the FSW tool-design parameters with regard to the welding strength of the joints.10–13 R. Kumar et al.14 experimen- tally studied the wear characteristics and defects after the FSW of AA6061-T6 aluminium alloys using different tool rotational speeds and welding speeds. They con- cluded that the wear resistance of the FSW joints increased compared to the base material. 2 EXPERIMENTAL SET-UP In this research, the selected base materials were wrought aluminium AA7075-T6 and cast aluminium A384.0-T6 with a 6.35-mm thickness. Aluminium and its alloys have low densities and high strength-to-weight ratios. As a result, these materials are used in various fields.15,16 The wrought AA7075-T6 aluminium with a 6.35-mm thickness was purchased and machined to dimensions of (100 × 50 × 6.35) mm using a circular saw machine. The A384.0-T6 aluminium was cast as an ingot and machined to dimensions of 100 × 50 × 6.35 mm using a saw machine and lathe. The chemical composi- tions and mechanical properties of the parent materials were tested and tabulated in Table 1 and Table 2, respectively. Table 2: Mechanical properties of the base metals Base metals UTS(MPa) YS (MPa) Elongation (%) Hardness (HRB) AA7075-T6 581.1 379.8 11.7 92.0 A384.0-T6 102.0 - 1.0 35.8 Table 3: Welding parameters Process parameters Unit Sym- bol Levels -1.682 -1 0 1 1.682 Tool rotational speed min –1 N 600 680 800 920 1000 Welding speed mm/min S 30 35 40 46 50 Axial load kN F 6 6.8 8 9.2 10 A design matrix was developed using the MINI- TAB-17 software with 3 variables and 5 levels. The welding parameters, or the variables selected for this research, were the tool rotational speed in min–1, the welding speed in mm/min and the axial load in kilo newton. These are shown in Table 3. After making different FSW welds as per the design matrix, the ultimate tensile strength (UTS) was tested and its values were tabulated in Table 4. As seen in Table 4, the minimum UTS for Run Number 5 was 246.33 MPa. The maximum UTS for Run Number 10 was 277.37 MPa. These two FSW welds were taken for further analysis of the wear resistance; Runs 5 and 10 were also re-designated as W-1 and W-2, respectively. The wear rates for W-1 and W-2 were K. ANGANAN et al.: EXPERIMENTAL STUDY AND ANALYSIS OF THE WEAR PROPERTIES OF ... 202 Materiali in tehnologije / Materials and technology 52 (2018) 2, 201–205 Figure 2: FSW process principle6 Figure 1: FSW machine Table 1: Chemical compositions of the base metals Metals/ elements Mg Mn Pb Zn Fe Cu Si Cr Ni Al AA7075-T6 2.29 0.047 0.004 5.44 0.20 1.45 0.071 0.24 0.006 Balance A384.0-T6 0.11 0.24 0.54 1.83 0.96 1.54 10.15 0.031 0.099 Balance analysed and compared with the wear resistance of the parent materials, viz., AA7075-T6 and A384.0-T6. The removal of the material from the solid surfaces of a solid-state contact is known as the wear. Table 4: Design matrix and the UTS results in MPa Run no. Design matrix FSW process parameters UTS N F S MPa 1 -1 1 -1 252.80 2 0 0 0 272.96 3 1 -1 -1 260.22 4 1 -1 1 255.85 5 -1 -1 -1 246.33 6 1 1 -1 267.80 7 1.682 0 0 261.76 8 -1.682 0 0 248.06 9 0 0 -1.682 260.60 10 1 1 1 277.37 11 0 1.682 0 264.02 12 -1 -1 1 252.37 13 0 0 1.682 271.67 14 -1 1 1 260.94 15 0 -1.682 0 248.31 16 0 0 0 271.00 17 0 0 0 271.90 18 0 0 0 272.00 19 0 0 0 272.10 20 0 0 0 271.80 The wear occurs on the outer surfaces of compo- nents. In this research, the pin-on-disk wear-testing me- thod was adopted. The pin-on-disk wear-testing appara- tus is shown in Figures 3 and 4. During this tribological test, a stationary disk rubs against the rotating pin while the applied load is constant.17 For the normal load range, the frictional-force range of the pin-on-disk apparatus was up to 200 N. The sliding speed was 0.26–12 m/s and the disk speed was 100–2000 min–1. The wear-disk diameter was 165 mm and it was made of the En31 material having a disk hardness of 58–60 HRC. The wear-disk track diameter ranged from 10 mm to 140 mm. The specimen-pin diameter ranged from 3 mm to 12 mm and the length of the specimen pin ranged from 25 to 30 mm. The dimensions of the specimen prepared for this research were (30 × 12 × 6.35) mm; the specimen consisted of the base metals AA7075-T6 and A384.0-T6. In the case of the dissimilar combination, the minimum and maximum UTSs were obtained for welded plates W-1 and W-2, whose weld-nugget areas were used as specimens for the wear test. The experimental wear tests were conducted under dry sliding conditions at normal atmospheric temperature and pressure. Figures 5 and 6 depict the respective wear-test specimen. 3 RESULTS AND DISCUSSIONS While conducting the wear test, the time and the revolution per minute of the disc were kept constant at 300 s and 500 min–1, respectively. By varying the mate- K. ANGANAN et al.: EXPERIMENTAL STUDY AND ANALYSIS OF THE WEAR PROPERTIES OF ... Materiali in tehnologije / Materials and technology 52 (2018) 2, 201–205 203 Figure 3: Pin-on-disk wear-test apparatus Figure 4: Pin-on-disk wear-test apparatus Figure 6: Specimen after the wear test Figure 5: Specimen before the wear test rial and the applied loads, the magnitude of the wear in microns was tabulated in Table 5. Using the above table, on the basis of the same applied loads, the materials were segregated and the wear values in microns were discussed. The materials at a 20-N load were grouped in one category and shown in Figure 7 as a bar chart. In this bar chart, the X-axis represents various materials and the Y-axis represents the wear in microns. The wear of the base material A384.0-T6 is higher than that of the base material AA7075-T6 or that of welds W-1 and W-2. This is because the hardness of the base material AA7075-T6 has a high hardness of 92 HRB, whereas the base material A384.0-T6 has a low hardness of 35.8 HRB. The materials at a 40-N load were grouped in another category and shown in Figure 8 as a bar chart. In this case, the wear of A384.0-T6 is also higher than that of the base material AA7075-T6 or that of dissimilar weld combinations of AA7075-T6 and A384.0-T6. The materials at a 60-N load were grouped as the third category and shown in Figure 9 as a bar chart. In this case, the wear of A384.0-T6 is also higher than that of the base material AA7075-T6 or that of dissimilar weld combinations of AA7075-T6 and A384.0-T6. The wear values for the base material AA7075-T6 and dissimilar friction-stir weld W-2 are more or less the same. K. ANGANAN et al.: EXPERIMENTAL STUDY AND ANALYSIS OF THE WEAR PROPERTIES OF ... 204 Materiali in tehnologije / Materials and technology 52 (2018) 2, 201–205 Table 5: Wear values Sl.no. Material min–1 Load (N) Time (s) Slidingvelocity Wear in microns COF average Frictional force (N) average 1 7075 500 20 300 3.141 m/s 27.34 0.4469 8.93 2 7075 500 40 300 3.141 m/s 43.07 0.3768 15.07 3 7075 500 60 300 3.141 m/s 38.17 0.3538 21.23 4 W-1 500 20 300 3.141 m/s 70.01 0.508 10.16 5 W-1 500 40 300 3.141 m/s 55.16 0.3451 13.80 6 W-1 500 60 300 3.141 m/s 50.56 0.2817 16.90 7 W-2 500 20 300 3.141 m/s 50.03 0.1452 2.90 8 W-2 500 40 300 3.141 m/s 50.19 0.2725 10.90 9 W-2 500 60 300 3.141 m/s 38.39 0.3088 18.53 10 384 500 20 300 3.141 m/s 90.51 0.345 6.90 11 384 500 40 300 3.141 m/s 63.77 0.4156 16.62 12 384 500 60 300 3.141 m/s 62.46 0.3354 20.12 Figure 10: Material wear at (20, 40 and 60) NFigure 7: Wear in microns at a load of 20 N Figure 9: Wear in microns at a load of 60 N Figure 8: Wear in microns at a load of 40 N Figure 10 shows the wear in microns of the base material AA7075-T6, welds W-1, W-2 and the base material A384.0-T6 with the applied loads of 20, 40 and 60 N. In the case of the base material AA7075-T6 at the applied loads of 20, 40 and 60 N, the wear was higher at the load of 40 N. In the cases of dissimilar welds W-1, W-2 and the base material A384.0-T6, the wear was reduced if the applied load was increased. This may be due to the increase in the temperature during the wear of the materials. 4 CONCLUSIONS The wear is one of the major mechanical properties of any material. In this research, the base materials were AA7075-T6 and A384.0-T6 aluminium alloys. The wear was discussed and analysed based on the analyses of dissimilar welds combining the AA7075-T6 and A384.0-T6 aluminium materials. The AA7075-T6 aluminium alloy had a high hardness of 92 HRB and the A384.0-T6 aluminium alloy had a hardness of 35.8 HRB. The hardness of FSW welds was between 35.8 and 92 HRB. At the same time, the wear was higher for the A384.0-T6 aluminium alloy and lower for the AA7075-T6 aluminium alloy. 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