I. ERTUGRUL et al.: FABRICATION OF MEMS-BASED ELECTROTHERMAL MICROACTUATORS WITH ADDITIVE ... 665–670 FABRICATION OF MEMS-BASED ELECTROTHERMAL MICROACTUATORS WITH ADDITIVE MANUFACTURING TECHNOLOGIES IZDELAVA ELEKTROTERMI^NIH AKTUATORJEV NA OSNOVI MIKRO-ELEKTRONSKO-MEHANSKIH SISTEMOV, IZDELANIH Z DODAJNIMI TEHNOLOGIJAMI Ishak Ertugrul 1,2* , Nihat Akkus 2 , Huseyin Yuce 2 1 Mus Alparslan University, Faculty of Engineering and Architecture, Department of Computer Engineering, 49250 Mus, Turkey 2 Marmara University Faculty of Technology, Department of Mechatronics Engineering, Goztepe Campus, 34722 Kadikoy – Istanbul, Turkey Prejem rokopisa – received: 2019-01-30; sprejem za objavo – accepted for publication: 2019-03-27 doi:10.17222/mit.2019.027 This study aimed to fabricate a bidirectional electrothermal microactuator that can be produced with the conventional mi- cro-electromechanical system (MEMS) fabrication technique, using two-photon polymerization (2PP) and projection mi- cro-stereolithography (PμSL) methods and to compare these methods with each other. The electrothermal microactuator that can move in two directions was designed in accordance with determined criteria. Although the same design was used for the 2PP and PμSL methods, the supporting structures were not produced with the PμSL method. For the PμSL method, the actuator was produced by removing the supports from the original design. Although 2-μm-diameter supports could be fabricated with the 2PP method, it was not possible to produce them with the PμSL method. Furthermore, the 2PP method was found to be better than the PμSL for the production of complex, non-symmetric support structures. Keywords: MEMS, 2PP, PμSL, thermal actuator, 3D-printer Avtorji opisujejo {tudijo izdelave dvosmernega elektrotermi~nega aktuatorja s konvencionalno MEMS tehnologijo (angl.: Mi- cro-Electro-Mechanical System), dvofotonsko polimerizacijo (2PP) in metodami projekcijske mikro-stereolitografije (PμSL) in nato primerjavo med njimi. Elektrotermi~ni aktuator, ki se lahko giblje v dveh smereh, so oblikovali v skladu z vnaprej dolo~enimi kriteriji. ^eprav so tako pri metodi 2PP, kot pri metodi PμSL uporabili enak dizajn, podporne strukture niso izdelali z metodo PμSL. Pri metodi PμSL so aktuator izdelali tako, da so odstranili podpore iz originalnega dizajna. ^eprav se lahko podpore premera 2 μm izdela z metodo 2PP, le-teh z njo ni bilo mo`no izdelati. Nadalje avtorji ugotavljajo, da je za izdelavo kompleksnej{ih nesimetri~nih podpornih struktur metoda 2PP primernej{a od metode PμSL. Klju~ne besede: MEMS, 2PP, PμSL, termi~ni aktuator, 3D-printer 1 INTRODUCTION It is known that the MEMS fabrication techniques are highly complex and expensive. The demand for MEMS is increasing with the advancement of technology. There- fore, some facilitating and low-cost production tech- niques are needed. There are many processing steps and clean-room re- quirements for the fabrication of traditional MEMS de- vices. With the development of 3D micro-additive manu- facturing technologies, the production costs and processing steps of MEMS devices have been gradually reduced. According to these advancements, it is possible to produce MEMSs in atmospheric air without the need for many operations (e.g., photolithography) and clean rooms. Additionally, challenging production procedures, such as Lithografie-Galvanformung-Abformung (LIGA), used for some materials, are not needed due to 3D mi- cro-additive manufacturing techniques. Many companies have used the 2PP method with 3D devices. In particular, the Photonic Professional GT and Photonic Professional GT2 products of Nanoschribe have used the 2PP technique very well. It has been seen that nano-size production is possible with these devices. 1 MEMS devices produced with the 2PP method can be used as micro-fluids, 2 micro-mechanical systems, 3–5 opti- cal systems, 6,7 cell structures, 8 and biomedical devices. 9,10 The PμSL method is also used by many companies to- day. The NanoArch™ is a 3D micro-fabrication equip- ment based on the PμSL technology. Studies that have been performed with the PμSL method include mi- cro-sensors, 11,12 micro-fluids, 13 optical systems, 14,15 bio- medical devices, 16 and mobile phones. 17,18 General trends show that many MEMS devices that can be produced with conventional MEMS fabrication techniques can also be manufactured with 3D printers. Moreover, it is evident that 3D-printer methods are more advantageous than traditional MEMS methods regarding the process steps and costs. In this study, the 2PP and PμSL methods, which are 3D MEMS manufacturing techniques, were examined in Materiali in tehnologije / Materials and technology 53 (2019) 5, 665–670 665 UDK 620.1:681.527:338.32.053.4 ISSN 1580-2949 Original scientific article/Izvirni znanstveni ~lanek MTAEC9, 53(5)665(2019) *Corresponding author's e-mail: i.ertugrul@alparslan.edu.tr detail, and an electrothermal microactuator was fabri- cated with these methods. These two methods were com- pared with regard to the fabrication results. It is thought that this study will contribute to the literature in terms of fabricating a microdevice through the use and compari- son of different methods. 2 MATERIALS AND METHODS 2.1 Bidirectional electrothermal actuator design 2.1.1 Working principle The actuator in our study is defined as the U-type. Such actuators are generally composed of both thin and thick arms and have different designs. A U-type actuator is shown in Figure 1. In such actuators, voltage is ap- plied to the pads and the thin arm expands due to warm- ing. This event is based on the temperature differences between the thin and thick arms. There is a decrease in the electrical resistance due to the increase in the cross-sectional area of the thick arm. This situation causes a decrease in Joule heating. Due to warming, the expansion occurs in the thin arm. Thus, the thin arm is longer. The actuator’s movement occurs for these rea- sons. 19 The bidirectional MEMS-based electrothermal microactuator is designed to move in two directions, right and left. In order for the actuator to move to the right of this design, DC-1 voltage must be applied as shown in Figure 2. Thus, if the voltage is connected to the pad attached to the hot arm while the ground is con- nected to the pad attached to the flexure arm, the actuator moves to the right. If the actuator is expected to move to the left, DC-2 voltage should be applied as shown in Fig- ure 2. Since our design is symmetrical and the actuator is incapable of moving to the right and left simulta- neously, voltages DC-1 and DC-2 are not applied at the same time. The actuator will move to the right or left ac- cording to the user request. 2.1.2 Design conditions The lengths of the arm and flexure are of great im- portance for the actuator to move to the right and left. Our design was made in accordance with the following criteria: 19,20 • The flexure arm must be as thin as possible. • The flexure arm must not be thinner than the hot arms as the flexure arm can overheat and cause defor- mation. • The flexure must be long enough to allow the actua- tor to change directions. • The flexure must be long enough not to deform the actuator. As our actuator has a symmetrical structure, dimen- sioning and designing were performed for a single arm as shown in Figure 3. All the dimensions of our actuator are given in Ta- ble 1. These values were obtained with the measure- ments of the actuator made with the 2PP and PμSL meth- ods. The same design was used for both methods. However, since the supporting structures cannot be pro- duced with the PμSL method, the measurements related to the support are given in Section 3. Table 1: Actuator parameters Parameter Symbol Value Unit Hot-arm length Lh 250 μm Cold-arm length Lc 200 μm Flexure-arm length Lf 100 μm Actuator gap Lg 7.5 μm Hot-arm width wh 3μ m Cold-arm width wc 6μ m Flexure-arm width wf 3μ m Air-gap thickness t 4μ m Actuator thickness t 3μ m 2.2 2PP technology The 2PP method has been a widely-used technology in the production of 3D microstructures in recent years. The simplicity and quickness of the fabrication, the pro- I. ERTUGRUL et al.: FABRICATION OF MEMS-BASED ELECTROTHERMAL MICROACTUATORS WITH ADDITIVE ... 666 Materiali in tehnologije / Materials and technology 53 (2019) 5, 665–670 Figure 3: Bidirectional electrothermal microactuator dimensions Figure 1: U-type actuator 19 Figure 2: Working principle of a bidirectional electrothermal microactuator duction of complex structures, and the high resolution al- low this technology to be preferred over the others. Photopolymer materials are used with this method. 21 In order to fabricate an actuator with the 2PP method, a femtosecond (fs) pulsed laser light source is required. The working principle of 3D microfabrication using the 2PP method is shown in Figure 4. Near-infrared (NIR) fs pulses produced with a titanium (Ti) sapphire laser are transformed into visible ones with an optical parametric oscillator (OPO). In order to adjust the intensity of the beam, the light source must enter a neutral density filter (ND). The beam focuses on the sample to initiate poly- merization. The photosensitive resin is compacted be- tween two coverslips and mounted on a 3D piezoelectric scanning layer. The motion of the scanning layer is pre-programmed with a computer to generate different microstructures. To analyze the fabrication process, it is recorded with a charge-coupled-device (CCD) camera. 22 For the 2PP method, the material used in this study was the IP-S resin. Table 2 gives the properties of this material. Table 2: Material properties of the actuator fabricated with the 2PP method 23,24 Parameter Symbol Value Unit Density D 1.2 g/cm 3 Young’s modulus E 4.6 GPa Poisson’s ratio V 0.35 - Thermal conductivity kp 1.82 W/m.K Thermal expansion coefficient 0.98 μm/m.K Specific heat capacity C 29 J/kg.K Electrical resistivity R 2.9 μ. .m Refractive index N 1.48 - 2.3 PμSL technology PμSL is a versatile and cost-effective process that can be used to rapidly generate microlenses, microgrippers, microfluidics and microbeams with electrolysis or resin additives. Materials such as a curable photopolymer, polymer and nanoparticle composites are used with this method. This method starts by creating a 3D structure using computer-based design (CAD) software and then turns the structure into a set of mask images (digital mask). The working principle of PμSL is shown in Fig- ure 5. Each image represents a thin layer of the 3D structure. During a production cycle, a single image is displayed on the reflective liquid crystal display (LCD) panel. The image from the LCD is then reflected on the liquid surface. The whole layer (usually 5–30 μm thick) is polymerized. Once the layer has been solidified, it is re-immersed in the resin to allow a new thin layer of liq- uid to form. Repeating the loop creates a 3D micro- structure from a layer stack. 25 The properties of the photosensitive resin, which were specially developed for this printer and used in the fabrication of the actuator, are given in Table 3. Table 3: Material properties of the actuator fabricated with the PμSL method 26 Parameter Symbol Value Unit Density D 0.89 g/cm 3 Young’s modulus E 0.9 GPa Poisson’s ratio V 0.89 - Thermal conductivity kp 1.12 W/m.K Thermal expansion coefficient 0.41 μm/m.K Specific heat capacity C 38 J/kg.K Electrical resistivity R 1.12 μ. .m Refractive index N 5.48 - I. ERTUGRUL et al.: FABRICATION OF MEMS-BASED ELECTROTHERMAL MICROACTUATORS WITH ADDITIVE ... Materiali in tehnologije / Materials and technology 53 (2019) 5, 665–670 667 Figure 5: Schematic of the working principle of PμSL 25 Figure 4: Working principle of 3D microfabrication with the 2PP method 22 3 RESULTS AND DISCUSSION 3.1 Fabrication with the 2PP technology The bidirectional electrothermal microactuator, whose design is illustrated in Figure 6a, was fabricated utilizing a 2PP-technology-based Photonic Professional GT device. 27 There are supports to the arms and pads of this design. The number of supports to the arms is 17, the diameter is 2 μm and the height is 4 μm while the number of supports to the pads is 3, the diameter is 40 μm and the height is 4 μm. The dimensions of these sup- ports are given in Table 4. Some unsuccessful experi- ments were done before this design. Fractures occurred during the fabrication when the number of supports to the arms was low. According to the experiments, the av- erage distance between the supports should be 45 μm in order to avoid breakage. As the number of supports to the flexure arm is related to the cold arm, continuous fractures occurred in experimental studies. A side view of the actuator on a glass wafer is given in Figure 6b. According to experimental studies, the maximum value of the resolution of a 3D printer should be 1 μm. Other- wise, the supports cannot be fabricated precisely. If the supports are not printed correctly, they cause collapses and breaks of the actuator. Table 4: Dimensions of supports in the actuator Parameter Symbol Value Unit Pad-support diameter rps 40 μm Arm-support diameter ras 2μ m Support height hs 4μ m An image of the actuator fabricated with the 2PP method is given in Figure 7. This image was taken with the microscope of the 3D printer. 3.2 Fabrication with the PμSL technology The bidirectional electrothermal microactuator, whose design is illustrated in Figure 8a, was fabricated using a PμSL-technology-based NanoArch™ series de- vice. 28 The production of the supported design with this method was not possible for two reasons. First, the sup- ported structures represent the system as a 3D design. However, it is not possible to produce 3D structures with the devices of the BMF Technology Company based on the PμSL technology. Second, these devices have a reso- lution of 2 μm and can fabricate a minimum thickness of up to 3 μm. When the support structures are removed, as I. ERTUGRUL et al.: FABRICATION OF MEMS-BASED ELECTROTHERMAL MICROACTUATORS WITH ADDITIVE ... 668 Materiali in tehnologije / Materials and technology 53 (2019) 5, 665–670 Figure 6: a) CAD design of the actuator. The structures at the top of the design were designed as the support; b) fabrication structure and design on the glass wafer Figure 8: a) CAD design of the actuator. The support structures under the actuator are removed; b) for fabrication, the silicon wafer is coated with a sacrificial layer of silicon nitride Figure 7: Image of the actuator fabricated with the 2PP method (photonic professional GT device’s camera) shown in Figure 8a, it is possible to perform the fabrica- tion as the actuator design can be introduced to the de- vice (a PμSL-technology-based 3D printer) in two di- mensions. The silicon wafer is coated with a sacrificial silicon nitride layer, used to separate the actuator from the silicon wafer, as shown in Figure 8b. The image of the actuator produced with the PμSL method is shown in Figure 9. This image was taken with the microscope of the 3D printer. 4 CONCLUSIONS In this study, a bidirectional electrothermal micro- actuator, fabricated with the traditional MEMS tech- nique, was produced using the 2PP and PμSL methods, which are 3D-printer procedures. These methods are the most common procedures used with 3D-printer devices. When the experimental results were examined, it was observed that 2-μm-diameter supports were produced with the 2PP method. However, it was not possible to produce them with the PμSL method. The minimum structure that could be fabricated with the PμSL method was 3 μm in length. Structures smaller than 3 μm could not be fabricated. Besides, the support structures could not be produced with the PμSL method even when the diameters of the supports were 3 μm. The support struc- tures were then removed and a normal actuator produc- tion was performed. It was determined that the PμSL method was not suitable for complex structures. 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ERTUGRUL et al.: FABRICATION OF MEMS-BASED ELECTROTHERMAL MICROACTUATORS WITH ADDITIVE ... 670 Materiali in tehnologije / Materials and technology 53 (2019) 5, 665–670