{"?xml":{"@version":"1.0"},"edm:RDF":{"@xmlns:dc":"http://purl.org/dc/elements/1.1/","@xmlns:edm":"http://www.europeana.eu/schemas/edm/","@xmlns:wgs84_pos":"http://www.w3.org/2003/01/geo/wgs84_pos","@xmlns:foaf":"http://xmlns.com/foaf/0.1/","@xmlns:rdaGr2":"http://rdvocab.info/ElementsGr2","@xmlns:oai":"http://www.openarchives.org/OAI/2.0/","@xmlns:owl":"http://www.w3.org/2002/07/owl#","@xmlns:rdf":"http://www.w3.org/1999/02/22-rdf-syntax-ns#","@xmlns:ore":"http://www.openarchives.org/ore/terms/","@xmlns:skos":"http://www.w3.org/2004/02/skos/core#","@xmlns:dcterms":"http://purl.org/dc/terms/","edm:WebResource":[{"@rdf:about":"http://www.dlib.si/stream/URN:NBN:SI:doc-VEGWMHGN/575106a8-d0c5-4d14-aa27-884ebabd632f/PDF","dcterms:extent":"243 KB"},{"@rdf:about":"http://www.dlib.si/stream/URN:NBN:SI:doc-VEGWMHGN/ada8bb4d-ed0d-4c5b-8efe-5ddca83b5fdd/TEXT","dcterms:extent":"18 KB"}],"edm:TimeSpan":{"@rdf:about":"1998-2025","edm:begin":{"@xml:lang":"en","#text":"1998"},"edm:end":{"@xml:lang":"en","#text":"2025"}},"edm:ProvidedCHO":{"@rdf:about":"URN:NBN:SI:doc-VEGWMHGN","dcterms:isPartOf":[{"@rdf:resource":"https://www.dlib.si/details/URN:NBN:SI:spr-KC6O72BG"},{"@xml:lang":"sl","#text":"Acta chimica slovenica"}],"dcterms:issued":"2013","dc:creator":["Ban, Irena","Drofenik, Mihael","Ferk, Gregor","Makovec, Darko","Stergar, Janja"],"dc:format":[{"@xml:lang":"sl","#text":"številka:4"},{"@xml:lang":"sl","#text":"letnik:60"},{"@xml:lang":"sl","#text":"str. 750-755"}],"dc:identifier":["ISSN:1318-0207","COBISSID:17438998","URN:URN:NBN:SI:doc-VEGWMHGN"],"dc:language":"en","dc:publisher":[{"@xml:lang":"sl","#text":"Slovenian Chemical Society"},{"@xml:lang":"sl","#text":"Slovensko kemijsko društvo"}],"dc:subject":[{"@xml:lang":"en","#text":"Curie point"},{"@xml:lang":"sl","#text":"krom"},{"@xml:lang":"en","#text":"magnetic hyperthermia"},{"@xml:lang":"en","#text":"magnetic nanoparticles"},{"@xml:lang":"sl","#text":"magnetna hipertermija"},{"@xml:lang":"sl","#text":"magnetni nanodelci"},{"@xml:lang":"en","#text":"mechanical alloying"},{"@xml:lang":"sl","#text":"nanozlitine"},{"@xml:lang":"sl","#text":"nikelj"}],"dcterms:temporal":{"@rdf:resource":"1998-2025"},"dc:title":{"@xml:lang":"sl","#text":"Synthesis of chromium-nickel nanoparticles prepared by a microemulsion method and mechanical milling|"},"dc:description":{"@xml:lang":"sl","#text":"A chemical and a physical method have been applied for the preparation of chromium-nickel alloy nanoparticles. These particles were designed to be used for controlled magnetic hyperthermia applications. Microemulsions with Ni2+ and Cr3+ and/or NaBH4 as precursors were prepared using the isooctane/CTAB, n-butanol/H2O system. The samples of CrxNi1-x nanoparticles with the desired composition were obtained after the reduction of their salts with NaBH4 and afterwards heat treated in a TGA in a N2 atmosphere at various temperatures. The CrxNi1-x materials were also prepared by mechanical milling. Utilizing a ball-to-powder mass ratio of 20 : 1 and selecting the proper alloy compositions we were able to obtain nanocrystalline CrxNi1-x particles. Thermal demagnetization in the vicinity of the Curie temperature of the nanoparticles was studied using a modified TGA-SDTA method. The alloy's phase composition, size and morphology were determined with XRD measurements and TEManalyses"},"edm:type":"TEXT","dc:type":[{"@xml:lang":"sl","#text":"znanstveno časopisje"},{"@xml:lang":"en","#text":"journals"},{"@rdf:resource":"http://www.wikidata.org/entity/Q361785"}]},"ore:Aggregation":{"@rdf:about":"http://www.dlib.si/?URN=URN:NBN:SI:doc-VEGWMHGN","edm:aggregatedCHO":{"@rdf:resource":"URN:NBN:SI:doc-VEGWMHGN"},"edm:isShownBy":{"@rdf:resource":"http://www.dlib.si/stream/URN:NBN:SI:doc-VEGWMHGN/575106a8-d0c5-4d14-aa27-884ebabd632f/PDF"},"edm:rights":{"@rdf:resource":"http://creativecommons.org/licenses/by/4.0/"},"edm:provider":"Slovenian National E-content Aggregator","edm:intermediateProvider":{"@xml:lang":"en","#text":"National and University Library of Slovenia"},"edm:dataProvider":{"@xml:lang":"sl","#text":"Slovensko kemijsko društvo"},"edm:object":{"@rdf:resource":"http://www.dlib.si/streamdb/URN:NBN:SI:doc-VEGWMHGN/maxi/edm"},"edm:isShownAt":{"@rdf:resource":"http://www.dlib.si/details/URN:NBN:SI:doc-VEGWMHGN"}}}}