P. M. KUMAR et al.: EFFECT OF PIN PROFILES ON THE MECHANICAL PROPERTIES OF FRICTION-STIR-WELDED ... 3–9 EFFECT OF PIN PROFILES ON THE MECHANICAL PROPERTIES OF FRICTION-STIR-WELDED AA5383 AND AA7075 VPLIV OBLIKE TRNA NA MEHANSKE LASTNOSTI VRTILNO-TORNO VARJENEGA AA5383 IN AA7075 Pandy Madhan Kumar 1 , Veerabathiran Anbumalar 2* 1 Department of Mechanical Engineering, Sri Nandhanam College of Engineering and Technology, Tirupattur 635603, India 2 Department of Mechanical Engineering, Velammal College of Engineering and Technology, Rameswaram High Road, Madurai 625009, India Prejem rokopisa – received: 2019-03-13; sprejem za objavo – accepted for publication: 2019-09-08 doi:10.17222/mit.2019.056 Friction-stir welding (FSW) is an unyielding-state welding process developed by The Welding Institute, United Kingdom. FSW is mainly based on the tool geometry, process parameters and welding material. The tool geometry plays the principle role in obtaining desirable microstructures of the welds, improving the strength and fatigue resistance of the joints. Currently, friction-stir-welding tools are designed using the trial-and-error method. In this study, three different types of FSW tools are considered for the fabrication of butt joints from AA5383 and AA7075. Various tool profiles such as the cylindrical taper projection, cylindrical thread-pin projection and triangle-pin projection are considered in the present study. The pin profiles are assessed based on the weld quality during tensile tests and hardness tests conducted on welded samples. With the analysis, it is found that the triangular pin produces sound welds at an 800-min –1 speed, 20-mm/min feed and 4-kN load. Keywords: friction-stir welding, microstructure, tool-pin profile, tensile strength, hardness Vrtilno-torno varjenje (FSW) je proces varjenja, ki so ga razvili na In{titutu za varjenje v Angliji. Potek in karakteristike FSW dolo~ajo predvsem geometrija orodja, procesni parametri varjenja in material, ki ga varimo. Geometrija trna orodja ima pomembno vlogo pri doseganju `elene mikrostrukture zvara oz. pri izbolj{anju trdnosti in odpornosti proti utrujanju varjenega spoja. Zaenkrat oblikovanje orodij za FSW temelji na metodi preizkus/napaka. V {tudiji so avtorji ocenjevali vpliv treh vrst trnov FSW orodja pri izdelavi zvarnih spojev med plo{~ami iz dveh Al zlitin: AA 5383 in AA7075. Uporabili so naslednje profilne geometrije trna orodij: cilindri~no sto`~asto, cilindri~no z navojem in trikotno. Na osnovi nateznih preizkusov in merjenja trdote so ugotovili, da vse tri geometrije omogo~ajo izdelavo odli~nih zvarnih spojev. Na osnovi izvedenih analiz so ugotovili, da s trikotnim profilom trna orodja lahko izdelajo dobre zvare pri hitrosti vrtenja orodja 800 min –1 , njegovem pomiku 20 mm/min in obremenitvi (sili) 4 kN. Klju~ne besede: vrtilno-torno varjenje, mikrostruktura, profil trna orodja, natezna trdnost, trdota 1 INTRODUCTION The friction-stir-welding technique is a non-consum- able unyielding-phase welding, which permits an extensive scope of parts and geometries to be welded. W. Thomas and his social group at The Welding Institute, United Kingdom, conjured it in 1991. Friction-stir weld- ing is used in modern industries such as shipbuilding, aerospace, automobile production and other modern manufacturing industries. It is frequently used for non-heat treatable or powder-metallurgy aluminium alloys, to which fusion welding cannot be applied. Thus, the weld mechanism and the relations between the microstructure, mechanical properties and process parameters have recently become fundamental studies. A detailed observation of the material microstructure in the joint section shows that there is an area located at the core of the weld, called "the nugget", where the original grain and sub-grain boundaries appear to be replaced with fine, equally recrystallized grains characterized by a nominal dimension of a few micrometers. Friction-stir welding, a modern and an environment-friendly solid- state joining process is used for joining a family of relatively light materials, especially aluminium and its alloys. The effectiveness of such a joint is strongly de- pendent on the geometry of the tool, process parameters and welding material. The tool geometric parameters, such as the height, the pin shape and the shoulder surface of the head, have a large influence on both the metal flow and the heat generation due to friction. 28 During friction-stir welding, various stirrer geometries are used for producing AA6063-T1 butt joints. For this reason, we have to investigate the mechanical properties of a joint and compare them with the microstructure of the joint. It was reported that a rotational speed of 2000 min –1 and a welding speed ranging from 50 mm/min to 200 mm/min produced a good weld; mechanical properties such as the tensile strength and hardness of the joint were also investigated. 20 The right-screw- and left-screw-geometry stirrer designs provide for a sound joint with no blemish in the weld metal, exhibiting an increased joint strength, better than that of an aluminium-based metal. 7 Researchers also Materiali in tehnologije / Materials and technology 54 (2020) 1, 3–9 3 UDK 620.1:621.7:621.791 ISSN 1580-2949 Original scientific article/Izvirni znanstveni ~lanek MTAEC9, 54(1)3(2020) *Corresponding author's e-mail: dranbumalarv@gmail.com (Anbumalar Veerabathiran) investigated the effects of the tool geometry on dissimilar friction-stir welding of polyethylene-poly- propylene. 18 Four different pin profiles, including threaded cylindrical, squared, triangular and straight cylindrical ones were considered. The interaction effects of welding variables, including the rotational speed and traverse speed were also studied. In order to control the material flow, the tools used were equipped with a stationary shoulder. 14 Tensile tests and durometer hard- ness tests were carried out and a microstructure analysis was conducted for all welded joints. It was observed that the threaded-cylindrical-pin profile produced mechan- ically strong welded joints. 15 Tool-pin profiles were also examined to determine the influence of the shoulder geometry on friction-stir welding of 1-mm copper-DHP plates. Tool welds were formed using three different shoulder geometries including flat, conical and scrolled ones at a varying traverse speed and rotation of the friction-stir-welding tool. The flat-shoulder tool proved to be insufficient for the welds because several defects were found in all the weld samples. On the other hand, the scrolled-shoulder tool is more effective than the conical one for the pro- duction of defect-free welds. However, both geometries require the lowest rotational speed to evade internal defects. At the same welding parameters, superior grain refinement, higher hardness and better strength are achieved in weld nuggets also by means of a scrolled FSW tool. 12 Studies proved the influences of various rotational speeds and friction-stir-welding tool geomet- ries on the macrostructure, microstructure and joint strength. Four tool-pin profiles (a conical-thread pin, a cylindrical conical-thread pin, a stepped conical-thread pin and a flared Triflute-pin tool) and two rotational speeds, 600 min –1 and 800 min –1 , were used. The results indicated that the friction-stir-welding tool geometry considerably influences the material flow in the nugget zone and, consequently, the weld mechanical proper - ties. 26 The influence of the pin geometry on various pro- perties of friction-stir-welded samples made with tools with different pin profiles was proved. In the case of four-flute cylindrical-pin profiles, friction-stir welding could not be performed on an aluminium alloy. 5 It was found in a research that tool geometries such as the cylindrical geometry, cone geometry, left-screw geom- etry and right-screw geometry affect the weld properties at a welding speed of 50–200 mm/min and rotational speed of 2000 min –1 . The mechanical properties such as the tensile strength and hardness of a joint were also investigated and compared with the microstructure of the joint. The results show that the shapes of the left- and right-screw stirrer provided for sound joints with no voids in the weld metal and with an increased joint strength that was higher than that of the aluminium- based metal. 19 The effects of the shoulder geometry of a tool used for milling-machine friction-stir-welded joints of alumi- nium alloy 1100 on the microstructural evolution and mechanical properties were studied. Three designs of the shoulder geometry were evaluated to induce different distributions of thermal cycles in the welding regions. Thermal cycles were measured using thermocouples and a data acquisition system. The system results showed that the featured shoulder tools produced an important effect on the thermal cycles, generating a wide plasti- cized region and the biggest grain size in the stir zone when compared with the flat-shoulder tool. 32 Resear- chers studied the production to forecast the ultimate tensile strength and hardness of the weld zone with and without tool profiles. The response-surface methodology deals with the movement of the material flow in friction-stir-welded aluminum alloy 6082. 9 The effects of important welding parameters and tool properties that affect the static strength of the friction-stir spot welds of polymer sheets were determined. Different tool-pin profiles, pin lengths and pin angles were used to produce the joints. Based on the experiments, the effects of the pin profile, pin length, pin angle and tool ro- tational speed on the friction-stir spot-welding formation and weld strength were determined for a specific alloy. 6 Improved heat-generating models for straight- and tapered-shoulder geometries with different tool-pin profiles for friction-stir welding were developed. They were developed by considering the welding process as a combination of pure sliding and pure sticking conditions. According to the results, the amount of heat generation is directly proportional to the number of edges in pin profiles so that the heat generated in the profiles increases from a triangular pin profile to a hexagonal pin profile. 33 Experimental relationships among the process parameters such as the rotational speed, welding speed and axial force help us envisage the maximum tensile strength. In addition, statistical tools, such as the cylin- drical-pin profile, are used for such investigations. 4 In a study on the geometry and size effects of sam- ples on the tensile properties of FSW AA 2024 joints, 2.5 times the tool shoulder is proposed for the gauge length. 9 Different tool designs and their effects are investigated and it is concluded that the pin profile is related to the mechanical properties and the maximum tensile strength is achieved for the cylindrical-pin profile with an 8-mm diameter. 34 Some studies also reported that samples made with a polygonal pin profile are hard and brittle in comparison with the cylindrical-pin-profile samples. 22 There are studies on the effects of three different tool geometries and two joint geometries on the quality of AA 5083-H111 T welds made with friction stir welding (FSW). All the tools have concave shoulders with diffe- rent pin geometries: a threaded taper pin, a quadrangular pyramidal and progressive pin, a partly threaded cylin- drical and partly pyramidal pin. T-lap and T-butt joint P. M. KUMAR et al.: EFFECT OF PIN PROFILES ON THE MECHANICAL PROPERTIES OF FRICTION-STIR-WELDED ... 4 Materiali in tehnologije / Materials and technology 54 (2020) 1, 3–9 configurations are also studied. The results show that no significant change in the hardness is observed with any combination of tool and joint geometries. The tensile- strength efficiency of the joints welded with the prog- ressive-pin tool was found to achieve the optimum level. 16 According to a study on the effects of tool design, new friction-stir-welding design features such as hollow, fluted and thermally insulated designs provide for a good welding thermal efficiency when compared to the conventional tool for aluminium welding. The effects of the tool-shoulder contact found during a thermal analysis of friction-stir welding are reported in 21 . The results show that the tool shoulder has a remarkable effect on the mechanical properties of AA6082. Observation revealed that the heat generation is higher between the trailing edge and retreating side-leading edge corner in the counter-clockwise direction and lower between the retreating side and the trailing edge in the clockwise direction. The results show that the welds produced with a ridge shoulder tool exhibit superior properties with a significantly lower axial force. 24 A literature review shows that the tool geometry is the most important parameter for achieving better weld- ing with friction-stir welding. It also shows that the tool geometry is selected based on the material to be welded. In the present work, three different types of tool geom- etry are considered for joining dissimilar aluminium alloys AA7075 and AA5383. 2 MATERIALS AND METHODS The welding materials used for modern investigations include aluminium alloys 5383 and 7075 whose chem- ical compositions are obtained using a vacuum spectro- meter. Aluminium alloy AA5383, also called Alloy 5S, is the major alloying element. Magnesium and silicon are the chief alloying elements; treatable precipitation- toughened aluminium alloy AA7075 contains zinc as the major alloying element. 27 Specimens of aluminium alloys AA7075 and AA5383 are used in the present study. The major alloying elements, magnesium and silicon, are found in precipitation-hardened aluminium alloy 7075. It is one of the universally used aluminium alloys, formerly called the 7-series alloy. Zinc as the most important alloying element is found in aluminium alloy AA5383. This alloy is strong and its strength is comparable to many steels. It was formerly called the 5-series alloy. The material properties of this alloy include a good fatigue strength, standard machin- ability and resistance to corrosion, which is better than those of the other aluminium alloys. The two aluminium alloys are used for the research. The chemical com- positions of AA7075 and AA5383 are shown in Table 1. They were analyzed with a vacuum spectrometer. 29 Table 1: Chemical compositions (%) of AA7075 and AA5383 Alloy AA7075 (%) AA5383 (%) Mg 2.374 4.237 Mn 0.028 0.579 Cu 1.564 0.012 Cr 0.251 0.064 Si 0.023 0.057 Al 90.05 94.78 2.1 Tool material Tool steel is one of the commonly used friction- stir-welding tool materials, allowing a weld of up to 50 mm. Here, welding deals with aluminium, copper and magnesium alloys. 1 Tool materials exhibit excellent machinability and thermal-fatigue resistance. Tool steels might cause damage and deformation during friction-stir welding of aluminium alloys and other low-melting- temperature materials. Tool steel can be used to weld both similar and dissimilar materials as lap joints or butt joints. During the welding using a butt-joint arrange- ment, a harder, high-carbon, high-chromium tool has a remarkably excellent wear resistance amongst different tool steels. H13 is characterized by shock and abrasion resistance combined with red hardness. A triangular tool-pin profile is shown in Figure 1. This tool-pin profile has a high toughness and 5-% chromium content. High-chromium stainless steel has a very high corrosion resistance. The softer material is on the retreating side and the tool material is on the advancing side and thus the tool is given a slight offset from the butt interface towards the softer material. 25 Stainless steel, high-carbon high-chromium steel, high- speed steel, H13 and C40 materials have been joined with tool steels. This high-carbon, high-chromium-steel tool material is used in the present investigation and its chemical composition is given in Table 2. It is noted for its high dimensional stability in addition to a good wear resistance and excellent edge-holding capabilities. Table 2: Chemical composition of HCHCr Components C Mg Si Ni Mo Cr w/% 97.67 0.97 0.19 0.25 0.80 0.12 This composition hardens the material so that it can sustain the high temperature in the stir zone generated during friction stirring. The density of the material is 7.7–8.03 g/m 3 , the melting point is 1426 °C and its P. M. KUMAR et al.: EFFECT OF PIN PROFILES ON THE MECHANICAL PROPERTIES OF FRICTION-STIR-WELDED ... Materiali in tehnologije / Materials and technology 54 (2020) 1, 3–9 5 Figure 1: High-carbon high-chromium triangular tool-pin profile elastic modulus is 190–210 GPa. Dies, cutters, measur- ing tools and finishing rolls for tier-mill sand punches are commonly made of high-carbon high-chromium steel. 10 Plates of 50 mm × 100 mm are machined and used as the specimens. The tool material used is HCHCr, containing C, Mg, Si, Ni, Cr and Mo. These tools show high dimensional stability with added wear resistance coupled with excellent edge-holding qualities and, hence, they are selected for the present investigation. 17 The welded blank of AA7075 and AA5383 can be used in the automotive sector as well as the aerospace industry where a high strength-to-weight ratio is the most desir- able property. 13 Aluminium alloys of the 7xxx and 5xxx series are not easily weldable with the conventional techniques. The electrical-resistance technique is also used to weld a few aluminium alloys. However, these techniques require an extensive surface preparation and prevention of an oxide formation, which is quite difficult and, thus, this limits their use to specific applications. 8 The raw materials in the form of plates that are 50 mm wide, 100 mm long and 6 mm thick are machined using a milling machine to make them parallel. The clamping system of the friction-stir-welding machine, leading to uniformity of the gaps between the plates is of crucial importance. The thickness of the welding plates range from 0.5 mm to 10 mm and the experiments are carried out on the friction- stir-welding machine. 2.2 Experimental set-up One of the most important aspects of FSW is the exploitation of a readily available vertical milling machine; friction-stir welding involves a large welding axial force of about 2500 kN and a fixture with proper clamps is designed to prevent the movement of speci- mens. The friction-stir-welding machine has a capability of welding plates with a thickness of 0.5–10 mm. Aluminium-alloy welded joints require a vertical head attachment, accommodating high spindle speeds that vary between 200 min –1 and 4000 min –1 , powered by 22-kW AC motor and with axis-stroke length movements of 600 mm, 200 mm and 300 mm along the x, y and z axes, producing professional tool-pin profiles. Friction- stir-welding process parameter called the traverse feed rate of the worktable is controlled by the automatic feed system of the milling machine. A FSW process requires a data acquisition system with suitable equipment for acquiring relevant parameters and monitoring the process. Large forces that develop when a FSW tool pin plunges into a workpiece to be welded directly affect the base plate and cause the plates to drift apart. Hence, a rigid clamping fixture is essential to withstand the forces and prevent the extrusion of the plasticized material from the joint interface to the bottom of the joint. The thermal-expanding and buckling behavior that the plates encounter during normal FSW conditions can also be restrained by the clamping. In the present work, fixture components are fabricated from mild-steel plates. The base plate is prepared using mild steel, having a size of 200 mm × 160 mm × 10 mm and it is machined precisely to hold the clamping plates and stopper plate for the AA5383 and AA7075 workpieces with a thick- ness of 6 mm. The friction-stir-welding tool and welding parameters play a very important role, determining the weld-joint characteristic. The experiment involving the major factors affecting friction-stir-welding parameters and tool design such as the tool rotational speed, welding speed and axial force are considered. Various parameters together with their ranges are selected and presented in Table 3. The weld joints are prepared using the Computer Numerical Control software to maintain the consistency. The welds are made by joining both plates (100 × 50 × 6) mm to make a weld joint with a width of 100 mm and a length of 100 mm. Workpieces are clamped firmly on the machine table, with the backward tool tilted at an angle of 0° throughout the length of the weld. The friction-stir weld is initiated by positioning the FSW tool in such a position that the tip of the pin just touches the upper surfaces of the workpieces. Table 3: Optimum parameters for preparing a welded joint S. No. Axial load (kN) Tool rotational speed (min –1 ) Worktable feed (mm/min) 1 4 800 20 2 5 1000 25 3 6 1200 30 2.3 Tension test The weld is recognized and a two-inch mark is made to allow the measurement of the elongation before the test sample breaks under tension. 2 The tensile test is performed according to the IS 1608:2005 specifications on the welded samples in a universal testing machine with a capacity of 100 kN. The tensile-test pieces are prepared and tested for each weld joint to ensure consistency and the data obtained for the welded specimens is shown on Figure 3. P. M. KUMAR et al.: EFFECT OF PIN PROFILES ON THE MECHANICAL PROPERTIES OF FRICTION-STIR-WELDED ... 6 Materiali in tehnologije / Materials and technology 54 (2020) 1, 3–9 Figure 2: Fabricated friction-stir-welding machine fixtures 2.4 Hardness test Hardness tests are conducted for both base plates, namely aluminum alloys AA5383 and AA7075 and also at the stir zone. To determine the effect of the tem- perature on friction-stir welding, the hardness of the welded stir zone is studied. The hardness of the welded specimen is estimated according to the Rockwell hard- ness ASTM E8 standard. 3 RESULTS AND DISCUSSION The welded butt joints are tested mechanically by conducting an ultimate-tensile test and a hardness test used for identifying the best parameters and excellent friction-stir-welding tool-pin profile; welded joints are analyzed with a scanning electron microscope (SEM). In the present investigation, welding is done by maintaining both the welding speed and axial load as well as by varying the rotational speed and tool pin profiles individually. The welding is carried out for the two dissimilar aluminum alloys, namely AA7075 and AA5383, as shown in Figure 4. 3.1 Tensile examination In the present work, the operation process parameters such as the worktable feed, axial load and tool rotational speed are considered; in addition, the triangle, cylin- drical thread and cylindrical taper pins are used and their influence on the mechanical properties are investigated. The experiments conducted show that for the triangle-pin profile, the tensile strength obtained for an axial load of 4 kN is 592 MPa. The tensile strength is decreased by 33 % by increasing the axial load by 1 kN. It can be concluded that the material has high strength when the axial load is low. In the case of cylin- drical threaded tool, a similar observation can also be made as an increase in the axial load from 4 kN to 6 kN results in a decrease in the tensile strength from 183.1 MPa to 91.7 MPa. A similar observation is made for the cylindrical taper tool. The tensile-strength values ob- served for the cylindrical thread pin are 162.6 MPa, 75.1 MPa and 93.2 MPa for the loads of 4 kN, 5 kN and 6 kN, respectively Figure 5. Some researchers also used a square tool and reported a value of 211 MPa for a 700-min –1 tensile strength when welding aluminum alloys AA5383 and AA7075. 29 Similar tensile-strength values were obtained and reported for friction-stir- welded aluminum alloys. 3.2 Hardness The hardness ordeal conducted on the welded sam- ples are in table the hardness value of the weldments done using triangle pin profile such as 4 kN is 72 from investigation triangle tool profile is effective when compared to the cylinder thread and cylindrical taper tool pin profile. P. M. KUMAR et al.: EFFECT OF PIN PROFILES ON THE MECHANICAL PROPERTIES OF FRICTION-STIR-WELDED ... Materiali in tehnologije / Materials and technology 54 (2020) 1, 3–9 7 Figure 3: Tensile-test specimens Figure 4: AA5383-AA7075 welded specimens Figure 5: Tensile examination results Figure 6: Hardness results Thus it can be concluded that mechanical properties of the welded samples the researchers using square tool is reported as 70 HRB for 700 min –1 Rockwell hardness value of welded aluminum alloys 5383 and 7075 alloys. 29 Similar kind of hardness values is obtained and researcher reported friction stir welded aluminium alloys. Table 4: Hardness results S. No. Pin profile Applied load (N) Rockwell hard- ness (HRB) 1 Cylindrical thread 980.665 40 2 Cylindrical thread 980.665 36 3 Cylindrical thread 980.665 32 4 Cylindrical taper 980.665 38 5 Cylindrical taper 980.665 24 6 Cylindrical taper 980.665 21 7 Triangle 980.665 71 8 Triangle 980.665 65 3.3 Microstructure of AA7075 and AA5383 The surface of the welded area exhibits uniform grains; it is smooth due to proper welding, maybe also due to the presence of new stir grains, improving the hardness of the welding zone. The region difficult to identify in the microstructure shows evidence of the stir-zone grain content in the main zone. The micro- structure of the welded aluminum alloys shown in Figure 7 shows a proper and uniform fusion of the materials because of the high temperature in the heated zone. In the stir zone, we recognize a very increasing hard- ness value of the welded samples. The welding prog- ression is homogeneous and controllable. As seen in the figure, due to the result of the welding progression, bumpy surfaces developed, proving that small weld burrs can be observed on dissimilar aluminium alloys 5383 and 7075. In the weld-stir zone, small microcracks can be observed, which may be a result of the friction-stir- welding tool-pin profile. 4 CONCLUSIONS In this present investigation, FSW of AA5383 and AA7075 dissimilar joints was successfully accomplished using different parameters, namely the welding speed, axial load, tool rotational speed and tool-pin profile. The weld quality at various tool rotational speeds, axial loads and welding-table feeds was studied, with a special emphasis on the tool-pin profile. Based on the tool-pin profiles and their influence on the mechanical properties, it is found that the triangle-pin profile provides for better mechanical properties than the cylindrical taper and cylindrical thread-pin profiles. 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