Strojniški vestnik - Journal of Mechanical Engineering 66(2020)6, 395-407 © 2020 Journal of Mechanical Engineering. All rights reserved. D0l:10.5545/sv-jme.2020.6566 Original Scientific Paper Received for review: 2020-01-26 Received revised form: 2020-05-02 Accepted for publication: 2020-05-29 Peak Temperature Correlation and Temperature Distribution during Joining of AZ80A Mg Alloy by FSW -A Numerical and Experimental Investigation P. Sevvel1'* - S.D. Dhanesh Babu2 - R. Senthil Kumar1 1 S.A. Engineering College, Department of Mechanical Engineering, Chennai, India 2 St. Joseph College of Engineering, Department of Mechanical Engineering, Sriperumbudur, India A quadratic equation has been developed based on experimental measurements to estimate the peak temperature in the friction stir welding (FSW)process during the joining of AZ80A Mg alloys. The numerical simulation of the FSW process was performed by employing COMSOL software to predict and calculate the distribution of temperature on the various regions of the parent metal and the welded joints. The predicted and finite element analysis (FEA) simulating the results of the distribution of peak temperatures were found to be consistent with the experimental values. In addition to this, a parametric experimental investigation was conducted to identity the most influential process parameter that plays a significant role in the peak temperature distribution during FSW of AZ80A Mg alloy. Linear contributions by the input process parameters of FSW, namely traversing speed, rotating tool speed and axial force on the peak temperature were observed to be 32.82 %, 41.65 % and 21.76 %, respectively. Keywords: peak temperature, AZ80A Mg alloy, process parameter, friction stir welding, tool pin profile Highlights • An investigational analysis during joining of AZ80A Mg alloy was carried out to formulate a correlation to analyse the generation of peak temperature. • The domination and significance of several parameters of FSW process on peak temperature during the joining of AZ80A alloy was investigated experimentally and numerically. • A three-dimensional steady-state model for heat-transfer in a movable type coordinate was modelled and simulated to visualize the temperature distribution in the parent metal. • The significance test of the predicted model fit for maximum temperature was performed using Minitab tool based on analysis of variance (ANOVA), and it was observed that the developed model was perfectly ideal, as the value of F was quite larger and Prob > F value was lower by 0.05. • It was inferred that performing the FSW of AZ80A Mg alloys at the optimized combination of higher speeds of tool rotation, with the FSW tool traversing at low speeds and by applying larger values of the axial load will result in the generation of ideal peak temperature, which will eventually contribute to perfect bonding between the AZ80A Mg alloy plates to be welded, thereby resulting in sound quality weldments. 0 INTRODUCTION As one of the earth's lightest metal alloys, Mg alloys are widely preferred for a variety of applications, in particular for aerospace, structural, automotive, electronics, and shipbuilding sectors [1] and [2]. The promising characteristic features of Mg alloys, in particular, AZ80A Mg alloy, includes tremendous strength-to-weight proportions, exceptional machinability, outstanding sound-absorbing potential, uncomplicated recyclability, and excellent machinability have attracted and gained the attraction of numerous researchers, in recent decades [3] and [4]. Concurrently, joining magnesium alloys is a tough task, especially when carried out by employing conventional joining processes, which is mainly due to their high thermal potential, which leads to undesirable features, including unrefined microstructure, porosity, relentless fracture, soaring residual stress, etc., in the joints obtained by employing conventional techniques [5] and [6]. A solid-state category of joining process like friction stir welding (FSW) is effective in eliminating those various defects associated with the employment of conventional welding processes employed for joining of AZ80A Mg alloys [7] and [8]. During the process of FSW, a uniquely designed tool with shoulder-and-pin arrangement is plunged (at a desirable rotating speed) exactly at the centre of the joining butt edges of the two similar or dissimilar plates to be joined and is made to traverse continuously along the line of fabrication, as illustrated in the Fig. 1. During this joining process, heat is generated due to the friction between the tool shoulder surface and the workpiece surface. Due to this generated frictional heat, the material of the flat plates (kept for joining) *Corr. Author's Address: S.A. Engineering College, Department of Mechanical Engineering, Chennai - 600077, India, drsevvel@saec.ac.in 395 Strojniški vestnik - Journal of Mechanical Engineering 66(2020)6, 395-407 is softened and reaches the plasticized state. The flow of these softened plasticized materials to the other side occurs due to the stirring action of the tool pin and impact of traversing tool shoulder. As a result, the mixing of the plasticized materials happens on both sides of the line of the joint, while the tool traverses along this joint line and thereby leading to the formation of a joint, without melting the base metals. The employed tool is then slowed gradually from the line of joint; next, the workpieces are allowed to cool down and thus, a solid phase of bonding is attained between the workpieces [9] to [11]. Temperature generation and its distribution over the various regions during the FSW process have an invigorating impact on the microstructural features and mechanical features of the fabricated welds [12]. For example, a flow-segregated deformation model was proposed by Arbegast [13] to depict the circumstances during which the formation of volumetric defects occurs during the joining of metals by the FSW process. It was observed that the disproportionate flow of plasticized material arising due to generation of high FSW processing temperature results in the formation of flash, the collapse of stir zone, etc. Padmanaban et al. [14] devised an analytical procedure to anticipate the generation and distribution of temperature and flow of the plasticized metal during FSW of AA7075 and AA2024 Al alloys. It was recorded that the level of temperature escalates with the rise in the speed of rotation of that cylindrical tool and with the increase in the diameter of that cylindrical tool's shoulder. A 3-D-based model for the transfer of heat during the process of FSW was put forward by Song and Kovacevic [15]. The equations of control were solved using the methodology of finite difference, and an intermittent mesh of the grid was used to calculate the temperature levels. Chao et al. [16] devised the transfer of heat taking place during the FSW process into a constant state horizon value-based scenario and calculated the temperature levels on the FSW tool and workpiece. This analysis recorded that nearly 90 % to 94 % of the generated heat is transferred to the workpiece, and remaining heat stays with the tool. Even though, an essential need for deriving and implementing suitable strategies for control of temperature exists in order to fabricate sound, high quality, defect-free welds, there is no consistent conclusion on the relationship between the welding parameters with the peak temperature. In this study, the domination and significance of several parameters of FSW process on peak temperature during joining of AZ80A alloy were investigated experimentally and numerically. Tmax correlation for AZ80A magnesium alloy was developed, for the first time, to accurately predict the peak temperature in the FSW process using the Minitab tool. The distribution of temperature on the various regions of the workpiece (AZ80A Mg alloy) was simulated by a steady-state heat transfer numerical approach using Comsol software. The predicted and FEA simulated peak temperatures were validated against experimental temperature measurements. Finally, a numerical parametric study was conducted taking into consideration the various parameters namely welding speed, axial load, and rotational tool speed to identify the most influential parameter affecting the peak temperature in the FSW process. 1 EXPERIMENTAL 1.1 Material, Machine, Tool, and Experimental Setup The wrought alloy of magnesium AZ80A (flat plates of 5 mm thickness) was the metal of examination in this experimental and numerical investigation. The chemical composition of the investigated AZ80A Mg flat plates was found to contain various elements, namely Al, Mn, Cu, Ni, Zn, etc. in the proportions of 7.85 % Al, 0.37 % Mn, 0.052 % Cu, 0.51 % Fe, 0.70 % Zn, 0.049 % Ni, 0.12 % Si and the remaining element was Mg. The strength of this alloy was observed to be in the value of 330 MPa (Tensile), 230 MPa (Yield) and 11 % (elongation). The joining (butt joint) of the flat plates (thickness: 5 mm) of parent metal (AZ80A Mg) was carried out by using a congenitally contrived, pseudo-automatic nature of FSW machine, enclosed with a motor spindle of 5 kW capacity, together with a 400 mm x 810 mm table, which can traverse in three different axes at a dimension of 510 mm (longitudinally), 400 mm (horizontally and vertically). The FSW tool employed in this experimental work was fabricated using the M35 grade highspeed steel, and it has a cylindrical shaped stepped shoulder (outer shoulder diameter of 20 mm and 15 mm diameter inner shoulder), along with a tapered pin profile (4.75 mm length). The photographic illustration of the different views of the tool used in this experimental and numerical investigation is shown in Fig. 1. Thermocouples made of Al-Cr wire were used to measure the workpiece temperature during this joining of AZ80A Mg alloy by the employment of the FSW process. The adopted schematic arrangement and installation of the thermocouples at various locations 396 Sevvel, P. - Dhanesh Babu, S.D. - Senthil Kumar, R. Strojniski vestnik - Journal of Mechanical Engineering 66(2020)6, 395-407 on the AZ80A (parent metal) Mg alloy surface is illustrated in Fig. 2. Temperature measurement was taken in three categories viz.; a) top side 10 mm offset from the axial line, b) top side transverse axis, and c) bottom side axial line. Fig. 1. Photographs of the different views of the tool used in this experimental and numerical investigation 1.2 Experimental Design Scheme The impact of the several parameters on the peak temperature (Tmax) during the joining of AZ80A Mg alloy flat plates employing FSW process was analysed by the adoption of a three-factor and three-level investigational design (full factorial-based) concept. The details of these influential parameters together with their coded (F axial force; Fd tool's speed of traverse and S tool's rotational speed) and corresponding realistic investigational values are elaborated in Table 1. Table 1. Description of influential parameters (taken into account) together with their coded and corresponding investigational values during joining of AZ80A Mg alloy by FSW Significant criterion Denotation Coded levels 0 -1 Traversing speed Fd mm/s 3 1.75 0.5 Force F kN 5 i 4 3 Tool rotational speed S rpm 1000 750 500 A 2nd order equation of polynomial nature was employed to fit the results of the investigational work. The proposed equation interprets the impact and role of the above-mentioned influential parameters and their interplay on the response variable (namely peak temperature). The generalized structure of the developed model is described, as shown below: T = K0 + K1A + K2B + K3C + K12AB + K13AC + + K23BC + KjjA2 + K22B2 + K33C2, (1) where the anticipated response is indicated by T, model constant by K0, linear coefficients by K2, K1, K3, cross-product coefficients by K13, K12, K23, quadraticcoefficientsbyK22, K11, K33. The effectiveness of the model was analysed using the Minitab Software 397 Strojniski vestnik - Journal of Mechanical Engineering 66(2020)6, 395-407 and by the employment of the analysis of variance (ANOVA). 1.3 FEA Modeling of the FSW Process Differential equation-based issues can be tackled by approximating the issue using a numeric strategy [17] and [18]. In this experimental investigation, the proposed analytical model for joining AZ80A Mg alloy employing an FSW tool (having a stepped cylindrical shoulder and tapered pin geometry) was formulated by applying the Comsol Multiphysics heat transfer segment. Statistical modelling is the partition and segregation of a geometrical region into limited cardinal points and rudimental volumes [19] and [20]. In this proposed model, a precise estimation of the administering horizon conditions influencing every network point and their adjoining points were also specified. Results were also derived for these structures of equations, culminating from the above-mentioned approximations. It can be visualized that the geometrical domain is symmetrical about the weld line. Hence, it is acceptable to model and conceptualize any of the flat plates of the base metal during their FSW. The dimension of the AZ80A Mg alloy flat plates welded in this experimental work is 50 mm (width) x 100 mm (length). The flat plates of the parent metal (AZ80A Mg alloy) were attached with two perpetual dominions along the X-direction. The obtained computational domain through FEA analysis for the base material on our investigational work, Convection and surface-ambient radiation Infinite domain namely, AZ80A Mg alloy is graphically illustrated in Fig. 3. 1.4 Governing Equations and Numerical Scheme Usually, during friction stir welding, the travel of the FSW tool is along the line of the joint of the weld. The proposed models by various researchers were proven to have some complications, as they have considered the FSW tool as a movable source of heat [21] and [22]. However, in the present experimental work, a lateral concept of the system of movable coordinates was employed, and the coordinates were fixed at the axis of the FSW tool. Due to this transfiguration of coordinates, the problem of transfer of heat is converted into static conduction-convection scenario, which is unequivocal to the proposed model. Moreover, this strategy of considering a movable type coordinate in this proposed model eliminates the need for modelling the processes taking place around the region of the FSW tool pin, thereby making this proposed model simplified and effective. The equation representing the amount of transfer of heat taking place on the parent metal of our experimental investigation (i.e., AZ80A Mg alloy) in a movable type coordinate is, pCpvVT + V-(-kTV) = Q, (2) where the temperature being generated is indicated by T, the capacity of heat by Cp, the density being indicated by p, the conductivity of heat by K, and the travelling speed of tool by p. Infinite domain ........\ / T0 ^----Heat generation (Shoulder-workpiece) Heat generation (Pin surface) Symmetry surface (Bonding region) 398 Strojniški vestnik - Journal of Mechanical Engineering 66(2020)6, 395-407 Table 2. Various temperature-dependent properties of AZ80A Mg alloy considered in this experimental work Temperature [°C] 20 50 100 150 200 250 300 350 Thermal conductivity [W/(m-K)] 59.2 63.3 68.2 73.4 77.3 82.1 92.9 98.9 Specific heat [J/(kgK)] 0.975 1.032 1.076 1.105 1.125 1.141 1.155 1.165 Density [kg/m3] 1806 1801 1793 1786 1778 1770 1763 1755 Likewise, the equation that governs the generation of heat in the region of interaction of the shoulder of the FSW tool and the parent metal is as follows: Qshou (R3shou ^pin,max) (3) where the generation of heat in the shoulder of the FSW tool is indicated by Qshou, m represents the angular rotational speed of the FSW tool, contact shear stress by Tcon, the radius of the FSW tool shoulder being indicated by Rshou and R pin,max represents the maximum radius of the profile of tool pin. The probe of the employed tool consists of a taper cylindrical surface with a bottom radius of Rpinmm, top radius Rpinmax and probe height Hpin. The heat generation equation for the profile of FSW tool pin is, ncox __con ^pin 2 H cos a K -R. (4) where Qpin indicates the amount of generated heat in the pin of the tool, the height of the tool pin being indicated by Hpin and Rpinmin represents the maximum radius of the profile of tool pin. The topmost and bottom portions of the parent metal experience some heat loss, and this happens mainly due to surface to circling radiation, convection, etc. The interrelated equations defining the flux of heat of these regions are mentioned below: Qup = hUp(T0 - T)+ s -o • (T\mb - T4), (5) Qdown = hdown(T0 - T)+ s ' o • (T4amb - T4X (6) where the flux of heat on the upper side of base metal flat plates (in W/m2) by Qup, the flux of heat on the upper side of base metal flat plates (in W/m2) by Qdown, the temperature reference (in Kelvin) is represented as T0, the surface temperature of base metal flat plates by T (in Kelvin), surface emissivity by s, the Stefan-Boltzmann constant by o, the ambient temperature of air (in Kelvin) by Tamb and the transfer of heat coefficients of natural convection are indicated by hdown and hup. In this investigational analysis, the transfer of heat coefficients for the topside was considered to be 6.25 W/(m2K) and 12.25 W/(m2K) for the bottom-and topside of the workpiece, respectively. The various properties of the parent metal, i.e., Mg alloy (AZ80A), which are taken into account in this experimental analysis for framing the proposed model are described in Table 2. Similarly, Table 3 describes the various properties of the material used for fabricating the FSW tool (i.e., HSS M35 Grade) employed in this experimental work, for framing the proposed model. From the knowledge gained from the literature survey, it has been observed that for attaining precise results, more grid nodes have to be placed around the surrounding region of the employed tool pin. This is mainly because the range and magnitude of the tool pin profile surface are very much less when compared with that of the workpiece surface. The diagrammatic illustration of the placing of innumerable grid nodes around the region of the FSW tool pin, through the generation of non-uniform mesh, shown in Fig.4. Table 3. Various properties of FSW tool material (M35 Grade HSS) considered framing the proposed model Characteristics Value Poisson's ratio 0.28 Specific heat [J/(kgK)] 465 Density [kg/m3] 8140 Thermal conductivity [W/(m-K)] 26 Young's modulus [GPa] 207 Table 4. Description of the various essential parameters, including the size of the mesh required for the generation of the mesh in the proposed model Description of parameter Value No. of elements 35100 Ultimate size of the elements 2.5 mm Curvature factor 0.2 Superlative growth rate of elements 1.3 Minimal size of the elements 0.026 Table 4 portrays in detail the various essential parameters, including the size of the mesh required for the generation of the mesh in the proposed model. The mathematical models relevant to the transfer of heat taking place due to radiation; convection and conduction are developed using the steady-state transfer of heat, based on the interface of solids. During the computation process, if the estimated temperature approaches the point of melting of the Peak Temperature Correlation and Temperature Distribution during Joining of AZ80A Mg Alloy by FSW - A Numerical and Experimental Investigation 399 Strojniški vestnik - Journal of Mechanical Engineering 66(2020)6, 395-407 Fig. 4. Generated model geometry for FSW simulation Illustration of the placing of Innumerable grid nodes around the region of the FSW tool pin, through the generation of non - uniform mesh investigating material, then the input of heat produced from the tool is modified to zero. In this experimental work, the melting point of the base metal is lower, when compared with that of the amount of frictional heat achieved between the workpiece surface and tool. As a result, the proposed model has been framed in such a way that the generation of frictional heat is adjusted to the value of zero, whenever the simulation temperature indicates higher values or values equivalent to the melting point of the parent metal. More simply, it can be written as, q = 0; (T> Tmelt). 2 RESULTS AND DISCUSSIONS (7) In this experimental and numerical analysis, 30 experimental runs (inclusive of 3 centre point experiments of control) were performed. The various measurement values obtained from these experiments were employed to frame the analytical model, which represents the peak temperature as the FSW process respond to the in constants. The values of the peak temperature measured during the experimental analysis, along with the predicted and FEA simulated values, are described in Table 5. The actual model equation for predicting the peak temperature (Tmax) of the FSW magnesium alloy AZ80A is given in Eq. (8). T= 111.2 + 0.562 x Speed+90.7 x Force - - 125.0 x Feed - 0.000229 x Speed x Speed - - 6.50 x Force x Force + 12.16 Feed x Feed - - 0.0007 x Speed x Force + + 0.02373 x Speed x Feed+ + 4.73 x Force x Feed. 2.1 Experimental Validation of Tm (8) It has been observed that the variations between the predicted correlation and the obtained actual values and the simulated FEA values are neutral and comparably small. The simulated and anticipated values are found to be consistent with the actual values. The values of R2 for the maximum temperature are 0.9991 and 0.9888 for the simulated and anticipated values, respectively, which reveals the fact that the retrogression is eloquent, as indicated in Fig. 5a and b. 2.2 Significance Test of the Predicted Model The significance test of the predicted model fit for maximum temperature was performed using Minitab tool based on ANOVA. The investigations were performed at a 5 % level of significance and for a confidence level of 95 percent. The ANOVA outcomes for the predicted peak temperature are mentioned 400 Sevvel, P. - Dhanesh Babu, S.D. - Senthil Kumar, R. Strojniški vestnik - Journal of Mechanical Engineering 66(2020)6, 395-407 Table 5. Results of the experimental run design matrix Runs Force in axial upward Speed of tool Speed of tool Max. temperature [°C] direction [kN] traverse [mm/min] rotation [rpm] Experi-mental Predicted FEA Simu-lated 1 5 1.75 1000 415 411.17 424.89 2 3 3 750 220 224.31 225.91 3 3 0.5 500 267 278.94 273.14 4 5 0.5 500 373 360.44 383.12 5 3 0.5 750 360 350.36 367.46 6 4 1.75 750 325 321.33 331.24 7 4 1.75 1000 383 371.33 391.49 8 3 1.75 500 186 189.50 192.91 9 3 1.75 750 257 268.33 263.33 10 5 1.75 750 368 361.33 381.39 11 5 3 750 331 329.14 337.89 12 5 0.5 750 429 431.53 440.96 13 4 0.5 750 398 397.44 409.74 14 4 1.75 750 323 321.33 331.24 15 3 0.5 1000 401 393.11 409.74 16 3 3 1000 273 281.89 282.36 17 4 3 1000 343 340.64 355.64 18 5 1.75 500 277 282.83 286.08 19 5 3 1000 390 386.39 398.74 20 4 0.5 500 331 326.19 342.81 21 4 0.5 1000 433 440.03 449.63 22 4 1.75 750 322 321.33 331.24 23 4 3 500 197 197.14 206.41 24 4 1.75 500 231 242.67 240.44 25 4 3 750 273 283.22 282.36 26 3 1.75 1000 319 318.50 331.24 27 3 3 500 163 158.06 165.89 28 4 1.75 750 325 321.33 331.24 29 5 3 500 237 243.22 244.96 30 5 0.5 1000 460 473.94 477.91 Peak Temperature Correlation and Temperature Distribution during Joining of AZ80A Mg Alloy by FSW - A Numerical and Experimental Investigation 401 Strojniški vestnik - Journal of Mechanical Engineering 66(2020)6, 395-407 Table 6. ANOVA results for peak temperature Source Degree of Freedom Seq SS Contribution [%] Adj MS Adj SS P-value F-value Effigy 9 176865 98.88 19651.7 176865 0.000 195.54 Linear 3 172129 96.23 57376.2 172129 0.000 570.92 Speed 1 74498 41.65 74498.0 74498 0.000 741.29 Force 1 38920 21.76 38920.5 38920 0.000 387.28 Feed 1 58710 32.82 58710.2 58710 0.000 584.20 Square 3656 2.04 1218.7 3656 0.000 12.13 Speed x Speed 1 1080 0.60 1408.8 1409 0.001 14.02 Force x Force 1 100 0.06 289.7 290 0.105 2.88 Feed x Feed 1 2475 1.38 2475.4 2475 0.000 24.63 2-Way interaction 1081 0.60 360.2 1081 0.032 3.58 Speed x Force 1 0 0.0002 0.3 0 0.955 0.00 Speed x Feed 1 660 0.37 660.1 660 0.019 6.57 Force x Feed 1 420 0.23 420.1 420 0.054 4.18 Error 20 2010 1.12 100.5 2010 Lack-of-Fit 17 2003 1.12 117.8 2003 0.004 52.37 Pure error 3 7 0.00 2.3 7 Total 29 178875 100.00 in Table 6 from which it can be observed that the developed model is perfectly ideal, as the value of F is quite larger and Prob > F value is lower by 0.05. Apart from this, it can also be visualized from this table that the linear contributions by the input process parameters of FSW namely, traversing speed, rotating tool speed and axial force on the peak temperature are 32.82 %, 41.65 %, and 21.76 %, respectively. Likewise, the square percentage contributions of these input parameters, namely, traversing speed, axial force and rotational speed on the peak temperature are 1.38 %, 0.06 %, and 0.60 %, respectively. These values reveal that the input parameter (i.e., the tool traversing speed) has a dominant part in influencing the peak temperature, during the joining of AZ80A Mg alloy. 2.3 Finite Element Temperature Distribution The predicted Tmax was verified with the observed temperature and was proved to agree with it perfectly. The optimized experimental conditions (rotational speed = 818 rpm; axial force = 3.646 kN; traversing speed of FSW tool = 1.48 mm/s) specified by Sevvel et al. [23] were taken into account for generating and drafting the line plots and contours. The variations of temperature in workpiece on the bonding line and the offset lines when the tool reaches mid of the work piece are shown in Fig. 6. The experimental outcomes are also compared with the FEA simulated values and included in this Fig. 6. — Distance 0 mm FEA - ■ - Distance 0 mm exp Distance 5 mm FEA — Distance 10 mm FEA - » Distance 10 mm exp — Distance 15 mm FEA VT — Distance 20 mm FEA -1- -t-1- k, -1- 0 20 40 60 SO 100 Longitudinal distance towards tool movement [mm] Fig. 6. Temperature variation along the longitudinal axis and its offset The comparisons aid in understanding that the FEA numerical results of the temperature values perfectly coincide with that of the experimental data. Also, the variations of the temperature in the workpiece transverse axis behind and in front of the tool movement were illustrated in Figs. 7a and 7b, respectively. It can be easily visualized from Fig. 8a and b that during the joining of AZ80A Mg alloy by FSW, the maximum value of temperature lies within the regions of workpiece contacted by the rotating FSW tool shoulder and is around 368 °C, which is nearly 70 % to 72 % of the melting point (490 °C) of the parent metal. 402 Sevvel, P. - Dhanesh Babu, S.D. - Senthil Kumar, R. Strojniški vestnik - Journal of Mechanical Engineering 66(2020)6, 395-407 ___ —Distance 0 mm FEA / \\ ---Distance 0 mm exp / \\ Distance 5 mm FEA / \ Distance 10 mm FEA -- • \ —Distance 15 mm FEA /yS^ ^""Ov —Distance 20 mm FEA --1-1-1-1-1-1-1-1-1- a) 10 20 30 40 50 —Distance0 mm FEA -■-DistanceO mm exp Distances mm FEA Distance 10 mm FEA —Distance 15 mm FEA —Distance 20 mm FEA b) Transverse distance infront of tool movement [mm] Fig. 7. a) Temperature variation along the transverse axis a) behind tool movement and its offset, and b) in front of tool movement and its offset The experimental results confirm that the FSW of Mg alloys (especially AZ80A Mg alloy) is a solidstate joining process and, during the fabrication of this Mg alloy joints, bonding has occurred perfectly, thereby resulting in sound quality welds. 2.4 Experimental Verification Using Optimized Values Fig. 9 shows the optical micrographs of the parent metal and various regions of the defect-free AZ80 Mg alloy FSW joints obtained during the employment of the optimized process parameters. From these optical micrographs, it can be visualized that the microstructure of the cast parent metal (AZ80A Mg alloy) consists of a dendritic network, with the cored grains of mg solid solution with large precipitates of Mg17Al12 particles at the grain boundaries, as shown in Fig. 9a. Fig. 9b portrays the region of the interface at the side of tool advancement. In this image, the left side shows the microstructure of the base metal, and the right side shows the zone of the nugget. This aids in perceiving that the impact of temperature and the stress has resulted in the uniform flow of zone of fusion along with the appearance of fragmented particles that have been recrystallized. The thermo-mechanically transformed region along with the constituents of the parent metals can be seen in Fig. 9c. This figure helps us to understand the orientation of grains from both the sides of the parent metal has taken place due to the impact of the peak temperature generated in the region of contact of the workpiece (i.e., the FSW tool shoulder surface) thereby resulting in the fusion of the constituents of the parent metal on both sides of the joint. Fig. 8. Temperature contour; a) obtained from FEA results for optimized condition, and b) on bonding surface for optimised condition (rotational speed = 818 rpm; axial force = 3.646 kN; traversing speed of FSW tool = 1.48 mm/s) We can also observe that the various surface regions of the parent metal closer to the contact point of the FSW tool shoulder region also have experienced a reasonable amount of heat generation and rise in temperature, which has led to the formation of alternate layers, as seen in the Fig. 9d, due to the marginal flow of plasticized material influenced by the stirring action by FSW tool shoulder. The impact of the peak temperature obtained during the joining of flat plates of AZ80A Mg alloy can be observed clearlyfrom Fig. 9e, which portrays us the partial evaporation of the constituents (mainly Zinc) from both the sides of the parent metal surfaces, which have been under the direct contact with the rotational shoulder of the FSW tool. Apart from this, we can infer that the FSW process also plays a very important role in improvising and enhancing Peak Temperature Correlation and Temperature Distribution during Joining of AZ80A Mg Alloy by FSW - A Numerical and Experimental Investigation 403 Strojniški vestnik - Journal of Mechanical Engineering 66(2020)6, 395-407 the microstructural characteristics of the magnesium alloys (especially AZ80A Mg alloy). This is evident from Fig. 9f, which shows the presence of fine fragmented grain particles, which have been spaced in a uniformly distributed homogeneous manner, when compared with the large, uneven, and coarse grains in the parent metal. This complete transformation of grain structure has occurred mainly due to the generation of ideal peak temperature resulting in super plasticity, uniform flow of the plasticized metal along with dynamic recrystallization. Fig. 9. Optical micrographs of; a) parent metal, b) region of interface at side of tool advancement, c) thermo-mechanically transformed region along with the constituents of the parent metal, d) regions of the parent metal closer to the contact point of the FSW tool shoulder region, e) shoulder influenced region with partial evaporation of constituents of base metal, and f) nugget zone of the defect-free AZ80 Mg alloy FSW joint obtained during the employment of the optimized process parameters To add additional weight to the inferred result of the complete transformation of grain structure due to the generation of the ideal peak temperature, the SEM image of AZ80A Mg alloy is shown in the Fig. 10a, which illustrates the presence of course, unevenly distributed with massive precipitates of Mg17Al12 particles at the grain boundaries. Fig. 10b portrays the interface region of the parent metal with the stir zone. This SEM image helps us understand that, at the interface region, the grains have been fragmented and, at the stir region, the constituents of the AZ80A Mg 404 Sevvel, P. - Dhanesh Babu Fig. 10. SEM images of the; a) parent metal, b) interface junction of the parent metal AZ80A Mg alloy with the stir zone, and c) centre of stir zone at 1000*magnification alloy have been completely dissolved, and the grains have been fragmented due to dynamic recrystallization. Fig. 10c shows the magnified SEM image of the stir zone obtained at 1000 x magnification. In this image, we can see the secondary phase particles of , S.D. - Senthil Kumar, R. Strojniški vestnik - Journal of Mechanical Engineering 66(2020)6, 395-407 the AZ80A Mg alloy has been completely dissolved, which occurred due to the generation of ideal peak temperature resulting from the adoption of optimized process parameters. 2.5 Influence of Process Parameters As it has been proved by several researchers [24] to [26] that the rotational speed of tool, its speed of traverse, and the load applied to it are some of the influencing parameters of an FSW process, in this experimental and numerical investigation, the influential role of those three process parameters on the peak temperature was analysed by simulating their impact during the impact on heat generation during the FSW of the parent metal, by employing the proposed FEA analysis model and are illustrated in the Fig. 11. From Fig. 11a, it can be inferred that the peak temperature escalates with the upsurge of the speed of rotation of the FSW tool and declines with the rise in the FSW tool's traversing speed. However, at the same time, from Fig. 11b, it can be interpreted that at the fixed tool traversing speed, with the simultaneous increase in the speed of rotation of FSW tool and axial load, the peak temperature rises. Moreover, at the fixed rotational speed of the FSW tool, the peak temperature escalates with the upsurge of the axial force and declines with the rise in the FSW tool's traversing speed, as shown in Fig. 11c. Based on the careful observation of these simulated temperature contour graphs, we can infer that performing the joining of AZ80A Mg alloys by FSW, at an optimized combination of higher rotational speeds of FSW tool, with the FSW tool traversing at low speeds and by applying larger values of the axial load results in the generation of ideal peak temperature, which eventually contributes to perfect bonding between the AZ80A Mg alloy plates to be welded, thereby resulting in sound quality weldments. 3 CONCLUSIONS In the present experimental research, an investigational analysis during the joining of AZ80A Mg alloy was carried out to formulate a correlation to analysis generation of peak temperature. The A3 dimensional steady-state model for heat-transfer in a movable type coordinate was modelled and simulated to visualize the temperature distribution in the parent metal. In addition to this, detailed parametric studies were carried out to understand the influence of parameters of the FSW process in the generation of Peak temperature [°C] 410.0 b) -2 I 1.0 1.5 2 0 2.5 Tool transverse speed [mm/s] Peak temperature [°C] I 2.5 3.0 3.5 4.0 4.5 5.0 Axial load [kN] Peak temperature [°C] I H 1.0 1.5 2.0 2.5 3.0 qJ Tool transverse speed [mm/s] Fig. 11. Simulated temperature contour on the bonding surface for optimized condition; a) concerning the speed of rotation of FSW tool and its traversing speed for fixed axial load, b) concerning the speed of rotation of FSW tool and axial load for fixed tool traversing speed, and c) concerning tool traversing speed and axial load at fixed speed of rotation of FSW tool peak temperature and the following inference were derived: • The formulated correlation for Tmax was able to accurately predict the maximum temperature generation during the FSW of flat plates of Peak Temperature Correlation and Temperature Distribution during Joining of AZ80A Mg Alloy by FSW - A Numerical and Experimental Investigation 405 Strojniški vestnik - Journal of Mechanical Engineering 66(2020)6, 395-407 AZ80A Mg alloy. The predicted Tmax was verified with the observed temperature and was proved to agree perfectly. • Variations between the predicted correlation and the obtained actual values and the simulated FEA values were found to be comparably small. The simulated and anticipated values are found to be consistent with the actual values. The values of R2 for the maximum temperature are 0.9991 and 0.9888 for the simulated and anticipated values, respectively. • Linear contributions by the input process parameters of FSW namely, traversing speed, rotating tool speed and axial force on the peak temperature were observed to be 32.82 %, 41.65 % and 21.76 %, respectively. Likewise, square percentage contributions of these input parameters, namely, traversing speed, rotating tool speed and axial force on the peak temperature are 1.38 %, 0.60 %, and 0.06 %, respectively. • The experimental and predicted values reveal that the input parameter (i.e., the tool traversing speed) has an important part in influencing the peak temperature during the joining of AZ80A Mg alloy. • The significance test of the predicted model fit for maximum temperature was performed using a Minitab tool based on ANOVA and it was observed that the developed model was perfectly ideal, as the value of F was quite larger and Prob > F value was lower by 0.05. • It was visualized from the generated temperature contour graphs that the maximum value of temperature lies within the regions of workpiece contacted by the rotating FSW tool shoulder and is around 368 °C, which is nearly 70 % to 72% of the melting point (490 °C) of the parent metal. • It was inferred that performing the FSW of AZ80A Mg alloys at an optimized combination of higher rotating tool speeds, with the FSW tool traversing at low speeds and by applying larger values of the axial load results in the generation of ideal peak temperature, which eventually contributes to perfect bonding between the AZ80A Mg alloy plates to be welded, thereby resulting in sound quality welds. 4 REFERENCES [1] Zhou, L., Nakata, K., Liao, J., Tsumura, T. 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