UDK 669.24:621.941:519.233.4 ISSN 1580-2949 Original scientific article/Izvirni znanstveni članek MTAEC9, 48(2)249(2014) OPTIMIZATION OF THE TURNING PARAMETERS FOR THE CUTTING FORCES IN THE HASTELLOY X SUPERALLOY BASED ON THE TAGUCHI METHOD OPTIMIRANJE SIL ODREZAVANJA S TAGUCHIJEVO METODO PRI STRUŽENJU SUPERZLITINE HASTELLOY X Abdullah Altin Van Vocational School of Higher Education, Yuzuncu Yil University, 65080 Van, Turkey aaltin@yyu.edu.tr Prejem rokopisa - received: 2013-04-23; sprejem za objavo - accepted for publication: 2013-06-11 In this study the effects of the cutting-tool coating material and cutting speed on the cutting forces and surface roughness were determined using the Taguchi experimental design. For this purpose, the nickel-based superalloy Hastelloy X was machined under dry cutting conditions with three different cemented-carbide tools. The main cutting force, Fz, is considered to be the cutting force as a criterion. The mechanical loading and the abrasiveness of the carbide particles have an increasing effect on the cutting forces. According to the results of the analysis of variance (ANOVA), the effect of the cutting speeds was not important. Depending on the tool-coating material, the lowest main cutting force was found to be 538 N and the lowest average surface roughness, 0.755 ^m, both at 100 m/min with a multicoated cemented-carbide insert KC9240, whose top layer is coated by TiN. Moreover, the experimental results indicated that the CVD cutting tools performed better than the PVD and the uncoated cutting tools when turning the Hastelloy X in terms of the surface quality and the cutting forces with the current parameters. Keywords: machinability, Hastelloy X, superalloy, cutting force, surface quality V tej študiji so s Taguchijevim eksperimentalnim sestavom določeni vplivi materiala oplaščenega rezilnega orodja, hitrosti rezanja na silo odrezavanja in hrapavost površine. V ta namen je bila superzlitina na osnovi niklja Hastelloy X obdelana pri suhih razmerah s tremi različnimi orodji iz karbidne trdine. Kot merilo je bila vzeta glavna sila rezanja Fz. Mehansko obremenjevanje in abrazivnost karbidnih delcev vplivata na povečevanje sile pri odrezavanju. Skladno z rezultati analize variance (ANOVA) vpliv hitrosti odrezavanja ni bil pomemben. Odvisno od prevleke na rezalnem orodju je bila ugotovljena najmanjša strižna sila 538 N in najmanjša povprečna hrapavost (0,755 ^m), oboje pri 100 m/min z večplastnim nanosom na vložku iz karbidne trdine KC9240 z vrhnjim prekritjem iz TiN. Rezultati poskusov so pokazali, daje pri struženju Hastelloy X s stališča kvalitete površine, sil pri rezanju pri danih parametrih CVD rezilno orodje boljše od PVD in od orodja brez prevlek. Ključne besede: obdelovalnost, Hastelloy X, superzlitina, sile rezanja, kvaliteta površine 1 INTRODUCTION in the clamshell of a rocket, engine tailpipes, afterburner components, cabin heaters, and other aircraft parts.4 It Nickel-based alloys constitute an important class of has also been found to be resistant in petrochemical materials that are used under demanding conditions of applications. Hastelloy X is widely used in a number of high corrosion resistance and high-temperature strength. industries.5 Wang,6 Richards and Aspinwall,7 Ezugwu These characteristics together with their good ductility and Wang,8 with Khamsehzadeh9 studied the effect of and ease of cold working make them generally very applied stress and temperatures generated at the cutting attractive for a wide variety of applications; nearly all of ^^ge and they were found to influence the wear rate and, which exploit their corrosion resistance in atmo1spheric, hence, the tool life. Notching at the tool nose and the salt water and various acidic and alkaline media.1Hastel- ^epth of cutting region was a prominent failure mode loy X is a nickel-chromium-iron-molybdenum alloy that when machining nickel-based alloys. This is due to a has been developed for high-temperature applications combination of high temperature, high workpiece and is derived from the strengthening particles, Ni2(Mo, Cr), which are formed after a two-step age-hardening strength,1^^ork hardening and abrasive chips. Kramer and heat-treatment process. With their face-centred cubic Hartung,10,11 observed that cemented-carbide tools used (FCC) structure, the Ni-Cr-Mo-W alloys, known as for machining nickel-based alloys at a cutting speed of Hastelloys, are used for marine engineering, chemical 30 m/min failed due to the thermal softening of the and hydrocarbon processing equipment, valves, pumps, cobalt binder phase and the subsequent plastic defor- sensors and heat exchangers.2 Hastelloy X is chosen by mation of the cutting edge. Focke et al.12 examined worn many for use in furnace applications because it has an tools, which revealed a layer of "disturbed material" unusual resistance to oxidizing, reducing, and neutral beneath the crater and the cutting edge. Hastelloy is a atmospheres. The resistance to localized corrosion ma- registered trademark name of Haynes International Inc. kes the alloy an attractive material as a general-purpose The Hastelloy trademark is applied as a prefix for a filler metal, or weld overlay.3 Hastelloy X is widely used range of corrosion-resistant nickel-based alloys promoted under the name "superalloys" or "highperformance alloys". Within corrosion applications, Hastelloy alloys may be chosen as a trade-off between performance, cost and other technical issues, e.g., suitability for welding. Hastelloy alloys are generally less attractive for use in acids compared to Tantaline (Tantaline is recognized as the leading performance/price option). Nomenclature v cutting speed (m/min) f feed (mm/r) da axial depth (mm) y tool life (min) Fm feed (mm/min) TL total length 2 MATERIALS AND METHOD 2.1 Experiment Specimens Specimens of Hastelloy X, which has an industrial usage, were prepared with dimensions of diameter 02 x 40 inches and then used for the experiments. The chemical composition and mechanical properties of the specimens are given in Tables 1 and 2, respectively. As the contents of the workpiece, chromium (21 %) and molybdenum (17 %), are high, the material is hard to machine. The material consists of approximately 50 % nickel, making the alloy suitable for high-temperature applications. The specimen was annealed and has a hardness of Rockwell B 90. ting forces (Fx, Fy, Fz). This allows direct and continuous recording and a simultaneous graphical visualization of the three cutting forces. The technical properties of the dynamometer and a schematic figure of the experimental setup are given in Table 3 and Figure 1, respectively. Table 1: Chemical composition of the workpiece material (Hastelloy X), w/% Tabela 1: Kemijska sestava obdelovanca (Hastelloy X), w/% Ni Cr Mo Fe Co W Mn Al Si C B 50 21 17 2 1 1 0.80 0.50 0.08 0.01 0.01 Table 2: Mechanical properties of Hastelloy X Tabela 2: Mehanske lastnosti Hastelloy X Hardness conductivit y(HB) Tensile strength (MPa) Yield strength (MPa) Breaking extension % (5 do) Thermal (W/m K) 388 1370 1170 23.3 11.4 Table 3: Technical properties of dynamometer Tabela 3: Tehnične lastnosti dinamometra Force interval (Fx, Fy, Fz) -5^10 kN Reaction < 0.01 N Accuracy Fx, Fy « 7.5 pC/N Accuracy Fz « 3.5 pC/N Natural frequency /o(x, y, z) 3.5 kHz Working temperature 0^70 °C Capacitance 220 pF Insulation resistance at 20 °C > 1013 Q Grounding insulation > 108 Q Mass 7.3 kg 2.2 Machine Tool and Measuring Instrument of Cutting Forces The machining tests were carried out on a JOHNFORD T35 industrial-type CNC lathe with a maximum power of 10 kW and a rotating speed between 50 r/min and 3500 r/min. During the dry cutting process, a Kistler brand 9257 B-type three-component piezoelectric dynamometer under a tool holder with an appropriate load amplifier was used for measuring three orthogonal cut- Figure 1: Measurement of the cutting forces and a schematic figure of the dynamometer unit Slika 1: Merjenje sil pri rezanju in shematski prikaz dinamometrske enote 2.3 Cutting Parameters, Cutting Tool and Tool Holder The cutting speeds (50, 65, 80, and 100) m/min were chosen by taking into consideration the ISO 3685 standard, as recommended by the manufacturers. The depth of the cut (1.5 mm) and the constant feed rate (0.10-0.15 mm/r) were chosen to be constant. During the cutting process, the machining tests were conducted with three different cemented-carbide tools, i.e., Physical Vapour Deposition (PVD) coated with TiN/TiCN/TiN; Chemical Vapour Deposition (CVD) coated with TiN+AL2O3-TiCN+TiN; and WC/CO. The dimensions of the test specimens were 2 x 40 inches in terms of diameter and length. The properties of the cutting tools and the level of the independent variables are given in Tables 4 and 5. Surtrasonic 3-P measuring equipment was used for the measurement of the surface roughness. The measurement processes were carried out with three replications. For measuring the surface roughness on the workpiece during machining, the cut-off and sampling length were considered as 0.8 mm and 2.5 mm, respectively. The ambient temperature was (20 ± 1) °C. The resultant cutting force was calculated to evaluate the machining performance. The following are the details of the tool geometry CNMG inserts when mounted on the tool holder: (a) CnMG shape; (b) axial rake angle, 6°; Table 4: Properties of the cutting tools Tabela 4: Lastnosti rezilnih orodij Coating material (top layer) Coating method and layers ISO grade of material _(grade)_ Geometric form Manufacturer and code Variables Level of variables Lower Low Medium High Cutting speed, v/(m/min) 50 65 80 100 Feed, f/(mm/r) 0.1-0.15 0.1-0.15 0.1-0.15 0.1-0.15 Axial depth, da/mm 1.5 1.5 1.5 1.5 CVD (TiN, Al2O3, TiCN, TiN, WC) P25-40, M20-30 CNMG120404RP Kennametal KC9240 PVD (TiN, TiCN, TiN, WC) P25-40, M20-30 CNMG120404FN Kennametal KT315 P25-40, M20-30 CNMG120404MS Kennametal K313 (c) end relief angle, 5°; and (d) sharp cutting edge. The cutting tool was mounted in the tool holder (PCLNR 2525M12) and used for such cutting tools (CNMG 120404) with an approach angle of 75°. Analysis of variance (ANOVA) was applied to the experimental study. Table 5: Level of independent variables Tabela 5: Nivoji neodvisnih spremenljivk Variables Cutting speed, v/(m/min) Feed, //(mm/r) Axial depth, da/mm Level of variables Lower 50 0.1-0.15 1 5 Low 65 0.1-0.15 1.5 Medium 80 0.1-0.15 1.5 High 100 0.1-0.15 1.5 3 RESULTS AND DISCUSSION 3.1 Cutting forces ai^^ s^^^ace ro^gh^ness After the test specimens were prepared for experimental purposes, they were measured with a three-component piezoelectric dynamometer to obtain the main cutting force. According to Figure 2, increasing the cutting speed decreases the main cutting force, excluding the area between 80 m/min and 100 m/min for K313. The lowest obtained values for the main cutting force at the cutting speeds of 50 m/min, 662 N, 65 m/min, 622 N, 80 m/min, 601 N, and 100 m/min, 538 N at a 0.1 mm/r constant feed rate, respectively. The lowest main cutting force was observed at 100 m/min cutting speed as 538 N. In Figure 2 the main cutting force depending on the cutting speed and the uncoating material of the cutting tool were changed in all the experiments. The cutting forces and surface roughness according to the experimental cutting parameters are given in Table 6. According to W. Konig, the cutting speed must be increased in order to reduce the main cutting forces.13 However, in this study, a decrease was observed in the main cutting force between 50 m/min and 100 m/min. It is thought that this case is caused by the good performance of the cutting tool. The effect of the TiN-coated carbide inserts was found to be important for the main cutting force, but the effect of the cutting speeds was not important in the analysis of variance. The main cutting force decreases in spite of increasing the cutting speed from 50 m/min to 100 m/min. As a result of the experimental data, an increase of 100 % in the cutting speed (from 50 m/min to 100 m/min), a decrease in the main cutting force with K313 (6.5 %), KT315 (10 %) and KC9240 (19 %) was found with the 0.1 mm/r constant feed rate, and the decreasing contact surface area caused the main cutting force to decrease in comparison to the increased cutting speed. The decrement of the cutting force depends on the material type, the working conditions and the cutting speed range.14 The high temperature for the flow region and the decreasing contact area and chip thickness cause the cutting force to decrease, depending on the cutting speed.15 As is widely known, the cutting speed must be decreased to improve the average surface roughness.16 The scatter plot between the surface roughness and the cutting speed as shown in Figure 3 indicated that there was a linear relationship between the surface roughness and the cutting speed. The results of Figure 3 show that the average surface roughness decreases by 66 % with an increasing cutting speed from 50 m/min to 100 m/min Figure 2: Change of main cutting force in Hastelloy X, according to the cutting speed: a) at f = 0.1 mm/r, b) at f = 0.15 mm/r Slika 2: Spreminjanje glavne sile rezanja materiala Hastelloy X pri hitrostih rezanja: a) f = 0,1 mm/r in b) f = 0,15 mm/r nt e mr ie ol to g in ut C ed e p s te rat) ut o pthm) e Fx/N Fy /N Fz /N ^a/um 1 K313 65 0.1 366 75 6Q1 1.7 2 K313 80 0.1 323 67 655 1.5QQ 3 K313 100 0.1 316 72 658 1.717 4 KT315 65 0.1 2Q5 132 622 1.605 5 KT315 80 0.1 281 130 601 1.41 6 KT315 100 0.1 277 130 5Q8 1.667 7 KCQ240 65 0.1 446 203 715 1.455 8 KCQ240 80 0.1 441 184 6Q4 1.368 Q KCQ240 100 0.1 3Q3 158 538 0.755 10 K313 65 0.15 3Q8 Q6 Q1Q 3.64Q 11 K313 80 0.15 371 Q0 Q01 3.462 12 K313 100 0.15 325 78 854 3.137 13 KT315 65 0.15 358 177 863 2.66Q 14 KT315 80 0.15 356 17Q 855 1.88 15 KT315 100 0.15 335 177 830 3.132 16 KCQ240 65 0.15 527 272 Q66 1.4Q2 17 KCQ240 80 0.15 446 187 6Q6 1.405 18 KCQ240 100 0.15 436 1Q5 6Q7 1.085 Figure 3: According to cutting speed the change of the average surface roughness in Hastelloy X: a) at f = 0.1 mm/r, b) at f = 0.15 mm/r Slika 3: Spreminjanje povpre~ne hrapavosti Hastelloya X od hitrosti rezanja: a) pri f = 0,1 mm/r in b) pri f = 0,15 mm/r Table 6: Cutting forces and surface roughness according to the experimental cutting parameters when turning Hastelloy X Tabela 6: Sile rezanja in hrapavost povr{ine pri ustreznih parametrih poskusa rezanja pri struženju Hastelloy X C o a ^ .3 ro g 1 10 11 12 13 14 15 16 17 18 13 n :3 C ) K313 K313 K313 KT315 KT315 KT315 KCQ240 KCQ240 KCQ240 K313 K313 K313 KT315 KT315 KT315 KCQ240 KCQ240 KCQ240 13 o a 65 80 100 65 80 100 65 80 100 65 80 100 65 80 100 65 80 100 0 1 0.1 0.1 0 1 0 1 0.1 0.1 0 1 0 1 0 15 0 15 0 15 0 15 0 15 0 15 0 15 0 15 0 15 ßi S ^ /N 366 323 316 2Q5 281 277 446 441 3Q3 3Q8 371 325 358 356 335 527 446 436 Fy /N 75 67 72 132 130 130 203 184 158 Q6 Q0 78 177 17Q 177 272 187 1Q5 Fz /N ^a/um 6Q1 655 658 622 601 5Q8 715 6Q4 538 Q1Q Q01 854 863 855 830 Q66 6Q6 6Q7 1 7 1. 5QQ 1. 717 1 605 1 41 1 667 1 455 1 368 0 755 3 64Q 3 462 3 137 2 66Q 1 8 3 132 1 4Q2 1 405 1 085 with the KCQ240 cutting tool (0 .1 mm/r constant feed rate) . 3.2 Optimization with the Taguchi Method In this part the optimization of the turning parameters was carried out in terms of the cutting forces with the Taguchi analysis The importance order of the effects of each control factor on the turning forces was identified For this purpose, the factors selected in the Taguchi experimental design and the levels of these factors are shown in Table 7 . Taguchi's L18 2*1 3*2 mixed design was used. In the Taguchi method there are three categories, i.e., "the smallest is better", "the biggest is better" and "the nominal is better" for the calculation of the signal/noise (S/N) ratio. In this research "smallest is better" was used since the minimum of the cutting force and surface roughness was intended. In the ;th experiment, the S/N ratio can be calculated using the following equation.17-1' 1 ^ 2 rj i =-10log1„ -1 Fi^ (1) n is the number of replications and Yi is the measured characteristic. Table 7: Cutting parameters and levels Tabela 7: Parametri rezanja in nivoji Control parameters Feed rate (A) Cutting speed (B) Cutting tool (C) Units m/min (mm/r) Levels 65 0.1 KC313 o 80 0.L5 KT3L5 100 KCQ240 3.3 Confirmation Experiments The final step of the Taguchi experimental design process includes confirmation experiments.18,1® To achieve this, the results of the experiments were compared with the predicted values using the Taguchi method and the error rates were obtained. The S/N ratios were predicted using the following model:18-20 k r pred = r „ (r - r „) (2) Moreover, the optimum turning parameters were obtained for the performance characteristics using the Taguchi analysis, where m is the total mean of the S/N ratios, i is the mean S/N ratio at the optimum level and k is the number of the main design parameters that significantly affect the performance characteristics. After predicting the S/N ratios other than 18 experiments (with Eq.2), the main cutting force or Fz was calculated using the following equation:20 Ypred =10 20 (3) 2 3 4 6 1 a Q where Fpred is the main cutting force or Fz with regard to the S/N ratio. 3.4 Taguchi Analysis for FZ Figure 4 shows the main effect plot for the S/N ratios, giving the effect of cutting parameters on the cutting force Fz. The smallest main cutting force is obtained with the cutting insert KT315. In this way, to achieve the minimum cutting forces it is understood that the KC9240 cutting tool should be used at a 0.10 mm/r feed rate and 100 m/min cutting speed. After analysing the effect of the cutting parameters on the cutting force, in order to find out which Fz cutting force it effected, a variance analysis was made. According to the results of the ANOVA in Table 8, it is understood that the most effective cutting parameters that effected the cutting force was 65.99 % and the cutting speed was 11.14 %. Table 8: ANOVA results for Fz Tabela 8: ANOVA-rezultati za Fz Main Effects Plot for SN ratios Source DF Sum of squares Mean square F Prob > F Distribution % A 1 181805 181805 57.75 0.002 65.99 B 2 30700 15350 4.88 0.085 11.14 C 2 13213 6607 2.1 0.238 4.80 A*B 2 4024 2012 0.64 0.574 1.46 B*C 2 9391 4696 1.49 0.328 3.41 A*C 4 23792 5948 1.89 0.276 8.64 Error 4 12592 3148 4.57 Total 17 275517 100.00 3.5 Taguchi Analysis for Ra Figure 5 shows the effect of feed rate, cutting speed and cutting-tool material on the average surface roughness. According to this figure, in order to obtain the smallest surface roughness, it is necessary to use the KC9240 cutting tool at a low feed rate (0.10 mm/r) and a Main Effects Plot for SN ratios Data Hsans 56 -57 3 ! ■58 I □ rflttf. [mm/reu.) _Cutting SoeeJ [m/min.l \ 0,10 0,15 fiS 80 iOO riiHingTnnl K313 KC92« KTSIS Signal-to-noiss; Smaller Is better Figure 4: Mean response graphs of the cutting forces according to the feed rate, cutting speed and cutting tool Slika 4: Prikaz odziva sil rezanja glede na hitrost podajanja, hitrost rezanja in rezilnega orodja I i: 1 i' -6 _riiTTirto _ \ 0,10 0,15 W so JOO Cjninc tool / S ion KC9240 Signsl-to-noise: Smaller is better »rnis Figure 5: Mean response graphs of the surface roughness according to feed rate, cutting speed and cutting tool Slika 5: Prikaz odziva hrapavosti povr{ine glede na hitrost podajanja, hitrost rezanja in rezilnega orodja high cutting speed (100 m/min). Besides this, in order to find out which important parameter affects the surface the roughness, the variance analysis was made with this aim. According to the results of the ANOVA in Table 9, the cutting parameters which effect the surface roughness, the cutting tool (40.38 %), feed rate, (33.15%) and 15.57 % feed speed and cutting tool's interaction were found. Table 9: ANOVA results for Ra Tabela 9: ANOVA rezultati za Ra Source DF Sum of squares Mean square F Prob > F Distribution % A 1 4.1424 4.1424 56.56 0.002 33.15 B 2 0.18817 0.09408 1.28 0.371 1.51 C 2 5.04646 2.52323 34.45 0.003 40.38 A* 2 0.06687 0.03343 0.46 0.663 0.54 B*C 2 0.81483 0.20371 2.78 0.173 6.52 A*C 4 1.94611 0.97305 13.29 0.017 15.57 Error 4 0.29294 0.07323 2.34 Total 17 12.49777 100.00 4 CONCLUSIONS The goal of this study was to identify the effect of turning parameters such as feed rate, cutting speed and cutting tools on the main cutting force and surface roughness using an analysis of Taguchi. The experimental design described here was used to develop the main cutting force and the surface-roughness prediction model for the Hastelloy X turning operation. The results of this experimental study can be summarized as follows: • The main cutting force decreased with increasing cutting speed and the cutting force increased at higher feed rates. • According to the analysis of Taguchi, in order to obtain the smallest cutting force and surface roughness, it was necessary to use the KC9240 cutting tool at a low feed rate (0.10 mm/r) and a high cutting speed (100 m/min). • The minimum main cutting force is obtained with CNMG 120404-type multicoated TiN+AL2O3-TiCN+ TiN carbide tools, while the maximum main cutting force is obtained as 965 N with the CNMG 120404-type uncoated carbide tools. However, cemented carbide tools have no significant effect on the main cutting force when machining Hastelloy X. • An increasing relation between the cutting speed and the arithmetic average surface roughness as well as between the coating number and the average surface roughness is observed. • In the case of coated tools, the effect of cutting speed on the surface roughness is no more pronounced than the effect of uncoated cemented-carbide inserts. • The minimum average surface roughness is determined with CNMG 120404-type multicoated TiN+ AL2O3-TiCN+TiN carbide tools, while the maximum average surface roughness is observed with CNMG 120404-type uncoated tools. Moreover, uncoated and multiple-layer coated tools have a significantly different effect on the average surface roughness. • It was found that there is a positive correlation between the main cutting force and the average surface roughness. 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